Development and Validation of a High-Performance Liquid Chromatographic Method for the Determination of Cinitapride in Human Plasma

Table 2

Recovery study.

S. no.	LQC response		MQC response		HQC response
	Extracted	Unextracted	Extracted	Unextracted	Extracted	Unextracted
1	110	116	459	543	1086	1170
2	94	119	496	549	1069	1176
3	116	120	483	551	1091	1182
4	89	114	492	542	1035	1172
5	92	109	469	549	1092	1169
6	100	116	491	551	1110	1183
Mean	100.16	115.66	481.67	547.50	1080.50	1175.33
SD	10.74	3.93	14.66	3.99	25.87	6.05
% CV	10.72	3.40	3.04	0.73	2.39	0.51
% recovery	86.60		87.98		91.93

LQC, 3 ng/mL; MQC, 15 ng/mL; HQC, 35 ng/mL of cinitapride.