Research Article

Simultaneous Quantification of Six Bioactive Components in Decoction of Ziziphi spinosae Semen Using Ultrahigh Performance Liquid Chromatography Coupled with Triple-Quadrupole Mass Spectrometry

Table 2

Calibration curves, correlation coefficients (r), and linear ranges of the six components.

AnalyteCalibration curverLinear range (μg/ml)LODs (ng/ml)LOQs (ng/ml)

Spinosiny = 2.08e6x + 7.35e50.999 60.197–6.3120.0390.118
6‴-Feruloylspinosiny = 1.32e6x + 3.79e50.999 70.184–5.8850.0920.276
Jujuboside Ay = 1.05e4x − 241.130.999 60.031–0.9913.1129.336
Jujuboside By = 7.28e4x − 2926.020.999 60.021–0.6682.1316.393
Camelliaside By = 1.10e7x + 6.01e50.999 70.020–0.6400.0990.299
Betulinic acidy = 1.00e7x + 9.11e50.999 80.141–4.5040.0710.213