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Journal of Analytical Methods in Chemistry
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Journal of Analytical Methods in Chemistry
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2018
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Article
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Tab 3
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Research Article
Optimization and Validation of Thermal Desorption Gas Chromatography-Mass Spectrometry for the Determination of Polycyclic Aromatic Hydrocarbons in Ambient Air
Table 3
Optimized conditions for thermal desorption system.
Primary desorption
Secondary desorption
Parameter
Parameter
Tube temperature
320°C
High trap temperature
320°C
Time
10 min
Low trap temperature
−10°C
Desorption flow
150 mL·min
−1
Time
6 min
Inlet split flow
23 mL·min
−1
Outlet split flow
10 mL·min
−1