Research Article

Optimization and Validation of Thermal Desorption Gas Chromatography-Mass Spectrometry for the Determination of Polycyclic Aromatic Hydrocarbons in Ambient Air

Table 3

Optimized conditions for thermal desorption system.

Primary desorptionSecondary desorption
ParameterParameter

Tube temperature320°CHigh trap temperature320°C
Time10 minLow trap temperature−10°C
Desorption flow150 mL·min−1Time6 min
Inlet split flow23 mL·min−1Outlet split flow10 mL·min−1