Simultaneous Analysis of Twelve Bile Acids by UPLC-MS and Exploration of the Processing Mechanism of Bile Arisaema by Fermentation

Table 1

Quantitative analytical results of Bile Arisaema in commercial (μg/g, n = 3).

Number	Origins	HDCA	CA	CDCA	HCA	GCDCA	GCA	GHDCA	TCDCA	THDCA	TCA	GHCA	THCA
20171201	Sichuan C&Y Traditional Chinese medicine Co., Ltd. (LOT.160109)	1950.70	27.61	2833.93	870.70	62.74	6.12	47.23	13.98	9.12	5.85	22.34	11.25
20171202	Sichuan C&Y Traditional Chinese Medicine Co., Ltd. (LOT.160101)	2121.04	29.19	3002.56	935.81	26.42	8.15	21.72	15.32	11.23	6.55	31.18	24.29
20171203	Sichuan C&Y Traditional Chinese Medicine Co., Ltd. (LOT.160601)	2101.06	33.45	3136.33	969.50	23.10	4.36	17.01	12.36	10.37	4.96	24.03	15.49
20171204	Sichuan Fuzheng Pharmaceutical Co., Ltd. (LOT.160509)	104.19	4.41	212.17	68.38	2.14	0.19	3.73	5.45	0.57	2.54	2.06	1.29
20171205	Sichuan Fuzheng Pharmaceutical Co., Ltd. (LOT.161206)	78.62	2.06	169.29	61.11	5.12	1.26	5.64	4.88	3.59	0.59	1.21	3.44
20171206	Sichuan Fuzheng Pharmaceutical Co., Ltd. (LOT.170108)	122.40	5.24	235.92	76.29	0.16	2.16	3.21	0.57	1.26	0.22	1.09	3.64
20171207	Neijiang Lianghui Pharmaceutical Co., Ltd. (LOT.170302)	ND	ND	ND	ND	ND	ND	2.68	ND	ND	ND	ND	ND
20171208	Beijing Tongrentang (Bozhou) Slice Co., Ltd. (LOT. 601002551)	326.73	2.75	155.33	178.06	2.58	1.26	0.59	4.22	3.87	0.34	4.25	3.51
20171209	Anhui Jiayu Traditional Chinese Medicine Co., Ltd. (LOT. 170206)	28.62	2.86	30.45	35.89	79.49	3.26	61.49	71.60	4.89	0.79	3.16	2.53
20171210	Beijing Huamiao Pharmaceutical Co., Ltd. (LOT. SBB2661)	834.94	6.53	1928.04	637.88	14.86	6.39	63.18	13.95	36.25	51.28	30.24	28.56
20171211	Beijing Huamiao Pharmaceutical Co., Ltd. (LOT. SB6191)	313.17	15.31	1048.05	295.01	5032.17	154.92	3436.47	750.92	258.18	197.53	146.55	164.23
20171212	Anguo Juyaotang Pharmaceutical Co., Ltd. (LOT. 1701002)	354.21	7700.96	1013.32	8327.74	43.26	328.29	132.1	562.37	78.16	1121.39	129.5	821.28
20171213	Sichuan Baisheng Pharmaceutical Co., Ltd. (LOT.170902)	4216.25	47.62	6386.69	2287.49	16.35	156.87	253.19	113.44	102.51	15.26	27.34	11.25
20171214	Sichuan Baisheng Pharmaceutical Co., Ltd. (LOT.171204)	839.32	21.16	1361.54	511.98	700.56	46.57	662.99	176.89	58.12	39.05	24.35	19.72
20171215	Sichuan Qianfang Traditional Chinese Medicine Co., Ltd. (LOT. 20170601)	4165.87	32.53	4444.88	1724.25	172.47	126.34	367.21	184.37	85.25	88.52	118.23	59.69
20171216	Sichuan Jianqu Pharmaceutical Co., Ltd. (LOT.170920)	2274.11	24.35	2133.02	1117.43	102.39	52.16	18.82	110.29	49.38	89.15	52.67	47.26
20171217	Yibin Traditional Chinese Medicine Co., Ltd. (LOT. 170501)	ND	5.45	ND	31.98	8.20	ND	9.05	ND	ND	ND	ND	ND
20171218	Sichuan Hongsheng Pharmaceutical Co., Ltd. (LOT.170903)	494.08	19.66	282.36	252.93	5.32	2.23	8.69	7.56	9.16	4.61	6.56	5.31
20171219	Sichuan Guanghan Traditional Chinese Medicine Co., Ltd. (LOT. 170411)	412.64	3607.23	918.88	3882.89	146.58	23.59	253.46	108.16	62.04	136.77	153.4	103.72
20171220	Beijing Qiancao Traditional Chinese Medicine Co., Ltd. (LOT. 170806)	660.79	536.16	1552.12	3818.08	100.23	55.61	165.24	253.97	176.24	248.56	236.12	118.55

ND: not detected.