Journal of Analytical Methods in Chemistry / 2019 / Article / Tab 4

Research Article

Quantitative Analysis of Eight Triterpenoids and Two Sesquiterpenoids in Rhizoma Alismatis by Using UPLC-ESI/APCI-MS/MS and Its Application to Optimisation of Best Harvest Time and Crude Processing Temperature

Table 4

Contents of the 10 investigated compounds in 42 batches of different RA dry temperature samples. AX: alismoxide, C alisol C 23C: alisol C 23-acetate, A alisol A 24A: alisol A 24-acetate, AL: alismol, B alisol B 23B: alisol B 23-acetate, 11-B: 11-deoxyalisol B 11-23B: 11-deoxyalisol B 23-acetate.

Sample no.AXC23CA24AALB23B11-B11-23B

Freeze-dried–10.0300.0740.1460.0330.0340.3930.6411.4890.2300.097
Freeze-dried–20.0300.0780.1790.0310.0390.4400.6261.4730.2010.120
Freeze-dried–30.0290.0850.1660.0390.0400.3910.6731.4200.2320.114
Freeze-dried–40.0320.0720.1630.0320.0440.3820.6321.4720.2420.115
Freeze-dried–50.0280.0840.1500.0330.0350.4300.5671.5800.2420.125
Freeze-dried–60.0320.0800.1610.0370.0340.4390.6191.5490.2200.109

60°C–10.0260.0690.1630.0420.0450.3620.5881.4130.2110.093
60°C–20.0280.0710.1690.0390.0460.4170.5961.3230.2000.103
60°C–30.0250.0590.1630.0370.0460.4030.6201.4770.2050.096
60°C–40.0260.0570.1500.0310.0440.3560.5771.3390.2160.101
60°C–50.0280.0630.1560.0470.0500.3960.5481.4120.1950.110
60°C–60.0240.0600.1630.0490.0410.3930.5711.3810.1770.099

70°C–10.0250.0550.1430.0450.0550.3410.5161.1790.1980.089
70°C–20.0270.0500.1540.0460.0500.3670.5641.3740.2060.086
70°C–30.0240.0550.1560.0460.0420.3770.5441.2480.1860.081
70°C–40.0250.0550.1480.0440.0490.3470.5701.1600.1970.089
70°C–50.0240.0490.1430.0500.0550.3720.5481.2650.1740.094
70°C–60.0240.0500.1540.0510.0440.3610.5281.1840.1900.079

80°C–10.0200.0370.1130.0850.1130.3030.4110.8810.1500.064
80°C–20.0190.0460.1280.0800.1430.2680.4560.9330.1390.068
80°C–30.0180.0440.1170.0820.1400.3040.4301.0170.1270.073
80°C–40.0160.0460.1200.0990.1160.3090.4910.8560.1310.062
80°C–50.0190.0390.1040.0750.1290.2960.4350.8230.1410.060
80°C–60.0210.0430.1210.0740.1200.2720.4740.8060.1400.057

100°C–10.0190.0390.0880.1310.1650.2450.3760.7060.1190.063
100°C–20.0180.0350.0830.1190.1850.2720.3050.7820.1070.071
100°C–30.0170.0380.0920.1210.1900.2410.3770.8300.1030.067
100°C–40.0150.0400.0850.1380.1660.2510.3620.7200.1150.059
100°C–50.0180.0350.0690.1010.1790.2330.4020.7630.0920.052
100°C–60.0200.0390.0920.1210.1570.2210.3490.8360.1010.055

120°C–10.0190.0320.0620.1160.3170.1930.2860.5660.0920.060
120°C–20.0180.0270.0780.1590.2960.2340.3140.6160.0880.056
120°C–30.0200.0350.0710.1510.3020.1960.2750.5700.0790.047
120°C–40.0210.0250.0830.1390.3600.2130.2920.6480.0950.063
120°C–50.0140.0290.0880.1280.2920.1890.3390.6950.0810.049
120°C–60.0190.0370.0620.1360.3530.1990.2820.6220.0820.050

150°C–10.0120.0280.0510.1690.4710.1370.2270.5220.0540.048
150°C–20.0100.0170.0700.1900.4230.1720.2410.4770.0670.054
150°C–30.0130.0120.0530.1530.4730.1650.1710.5050.0580.045
150°C–40.0100.0280.0500.1610.5210.1480.2250.4270.0510.048
150°C–50.0080.0220.0640.1490.4010.1680.2060.3750.0650.052
150°C–60.0110.0290.0600.1410.4600.1570.2210.5230.0490.048

We are committed to sharing findings related to COVID-19 as quickly and safely as possible. Any author submitting a COVID-19 paper should notify us at help@hindawi.com to ensure their research is fast-tracked and made available on a preprint server as soon as possible. We will be providing unlimited waivers of publication charges for accepted articles related to COVID-19. Sign up here as a reviewer to help fast-track new submissions.