Journal of Analytical Methods in Chemistry / 2019 / Article / Tab 7

Research Article

Optimization of Extraction Conditions for Determination of Tiliroside in Tilia L. Flowers Using an LC-ESI-MS/MS Method

Table 7

Tiliroside contents in extracts from Tilia L (±SD, ).

SamplesEfficiency of extraction (%)aContent of tiliroside (mg per g dry extracts)

MAC-E70%13.71.530 ± 0.001
MACst-H17.40.142 ± 0.005
MACst-E50%14.61.105 ± 0.010
MACst-E70%17.41.717 ± 0.005
MACst-E100%5.31.289 ± 0.002
MACst-E70% + AA0.5%18.55.010 ± 0.024
MACst-E70% + AA1%18.45.370 ± 0.033
MACst-E70% + AA2%20.12.870 ± 0.011
MACst-E70% + AA5%21.12.540 ± 0.010
MACst-E70% + AA10%19.52.990 ± 0.009
MACst-E70% + DE5%15.43.900 ± 0.013
MACst-E70% + DE10%13.23.560 ± 0.012
MACst-E100% + AA0.5%62.130 ± 0.008
MACst-E100% + AA1%62.160 ± 0.006
ASE-M100% (80)14.84.980 ± 0.037
ASE-M70% (80)22.34.440 ± 0.028
ASE-M50% (80)22.01.371 ± 0.013
ASE-CH100% (50)1.50.193 ± 0.001
ASE-E100% (80)3.36.810 ± 0.014
ASE-E70% (80)19.62.980 ± 0.007
ASE-E50% (80)8.82.320 ± 0.012
ASE-E70% (80) + AA0.1%23.03.200 ± 0.013
ASE-E70% (80) + AA0.5%18.95.160 ± 0.017
ASE-E70% (80) + AA1%26.47.400 ± 0.019
ASE-E70% (80) + AA5%27.81.802 ± 0.004
ASE-E100% (80) + AA0.5%18.95.850 ± 0.012
ASE-E100% (80) + AA1%10.85.560 ± 0.015
UR-E70%23.61.225 ± 0.006
UR-DE5.69.842 ± 0.028
UR-E70% + AA1%18.11.821 ± 0.010
UAE-M100% (rt)3.64.281 ± 0.084
UAE-M70% (rt)5.11.358 ± 0.016
UAE-M50% (rt)6.60.829 ± 0.004
UAE-E100% (rt)2.53.291 ± 0.059
UAE-E70% (rt)4.01.728 ± 0.028
UAE-E50% (rt)4.11.244 ± 0.019
UAE-M100% (80)9.42.116 ± 0.038
UAE-M70% (80)9.21.120 ± 0.019
UAE-M50% (80)5.41.650 ± 0.054
UAE-E100% (80)72.406 ± 0.001
UAE-E70% (80)7.51.607 ± 0.007
UAE-E50% (80)5.82.072 ± 0.015
UAE-E70% (80) + AA0.5%8.41.848 ± 0.004
UAE-E70% (80) + AA1%6.63.212 ± 0.021
UAE-E100% (80) + AA0.5%2.83.322 ± 0.012
UAE-E100% (80) + AA1%43.368 ± 0.057

aCalculated as percentage of dry extract obtained from 1 g of raw material.

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