Determination of Halogens by Ion Chromatography in Edible Mushrooms after Microwave-Induced Combustion for Sample Preparation

Table 2

Limits of detection and quantification for chlorine by IC and for bromine and iodine by ICP-MS, using different absorbing solutions for sample preparation of mushrooms (500 mg) by MIC.

Absorbing solution	LOD (mg kg^−1)			LOQ (mg kg^−1)
	Chlorine	Bromine	Iodine	Chlorine	Bromine	Iodine
Ultrapure water	9	0.005	0.008	17	0.019	0.012
50 mmol L^−1 NH4OH	10	0.040	0.014	18	0.069	0.016
100 mmol L^−1 NH4OH	40	0.066	0.014	74	0.096	0.015
150 mmol L^−1 NH4OH	Nd	0.068	0.014	Nd	0.099	0.016

Not determined.