Journal of Analytical Methods in Chemistry / 2022 / Article / Tab 5 / Research Article
Quality Evaluation of Decoction Pieces of Gardeniae Fructus Based on Qualitative Analysis of the HPLC Fingerprint and Triple-Q-TOF-MS/MS Combined with Quantitative Analysis of 12 Representative Components Table 5 The contents of the 12 components in 40 samples (mg/g).
No. Geniposide Genipin gentiobioside Gardenoside Shanzhiside DAAME SME Geniposidic acid Total of iridoidsa Crocin I Crocin II Jasminoside B Chlorogenic acid Rutin S1 56.157 17.254 3.324 1.616 0.279 0.240 0.288 79.159 7.733 0.879 1.184 0.175 0.452 S2 63.507 17.373 3.445 1.899 0.365 0.196 0.232 87.017 6.984 0.767 1.166 0.493 0.627 S3 47.306 8.479 3.230 0.767 0.214 0.174 0.137 60.308 7.640 1.156 0.794 0.437 1.043 S4 50.841 11.828 5.277 2.186 0.774 0.434 0.223 71.563 8.613 1.025 1.046 1.065 1.184 S5 49.480 10.326 5.043 2.159 0.821 0.452 0.246 68.526 8.122 0.905 0.956 1.386 1.315 S6 67.039 14.199 3.720 2.021 0.325 0.202 0.336 87.843 9.578 1.087 1.386 0.192 0.558 S7 57.153 20.159 3.293 1.405 0.622 0.297 0.412 83.341 6.061 1.251 1.023 0.187 0.595 S8 58.755 18.663 3.865 1.058 0.314 0.279 0.161 83.095 11.768 1.538 1.894 0.298 0.769 S9 56.628 20.945 3.687 1.737 0.277 0.183 0.244 83.701 5.586 0.909 0.947 0.275 0.536 S10 40.684 11.943 6.085 2.877 0.553 0.368 0.314 62.824 9.463 1.316 1.556 1.220 0.862 S11 49.570 12.767 3.688 1.487 0.479 0.348 0.189 68.526 8.798 1.226 1.259 0.152 0.492 S12 55.511 15.942 4.705 1.127 0.407 0.342 0.171 78.205 7.801 1.137 1.391 0.284 0.889 S13 45.203 8.848 6.438 2.488 0.802 0.256 1.499 65.534 9.038 1.578 0.949 1.900 0.478 S14 63.439 16.376 3.654 1.912 0.335 0.283 1.056 87.056 8.186 0.816 0.948 0.223 0.484 S15 57.478 14.724 2.873 1.854 0.335 0.259 0.166 77.690 10.132 1.200 1.377 0.137 0.514 S16 37.917 10.029 5.794 2.631 1.634 0.913 1.013 59.931 6.908 1.297 0.677 0.946 0.928 S17 50.662 16.733 2.693 0.936 0.565 0.404 0.132 72.124 5.735 0.777 0.562 0.566 0.491 S18 46.155 11.622 2.949 1.245 1.075 0.900 0.737 64.683 4.848 0.638 0.384 0.770 0.800 S19 46.483 9.444 5.048 2.334 0.447 0.327 0.170 64.253 9.612 1.667 1.411 0.667 0.936 S20 50.726 16.015 6.851 2.619 0.714 0.433 0.261 77.619 7.547 1.167 0.971 0.985 0.768 S21 47.560 16.348 6.315 2.257 0.872 0.551 0.250 74.153 7.438 1.055 1.086 0.734 0.665 S22 49.344 12.668 8.705 3.011 0.766 0.503 0.240 75.236 9.473 1.569 1.376 1.110 0.772 S23 61.648 15.332 3.138 1.005 0.541 0.200 0.169 82.033 11.266 1.334 1.352 0.456 0.475 S24 48.245 13.228 6.116 2.546 0.768 0.486 0.209 71.598 8.778 1.307 0.912 1.032 0.725 S25 51.362 10.919 5.128 1.502 0.527 0.368 0.256 70.062 6.948 0.952 0.790 0.476 0.742 S26 57.580 18.966 3.111 1.216 0.366 0.283 0.161 81.683 6.872 1.249 1.165 0.260 0.712 S27 50.456 13.112 3.050 1.777 0.455 0.264 0.130 69.244 10.195 1.564 1.214 0.175 0.531 S28 49.031 12.675 4.073 0.931 0.399 0.249 0.187 67.546 8.274 1.277 1.149 0.327 0.720 S29 51.922 10.231 3.632 1.167 0.469 0.348 0.277 68.045 7.475 1.024 0.920 0.618 1.007 S30 43.513 7.670 5.608 2.419 0.880 0.590 0.514 61.194 7.187 0.789 0.743 1.285 0.758 S31 54.676 9.316 4.095 1.180 0.598 0.378 0.347 70.590 6.558 1.202 1.238 0.624 1.601 S32 72.216 6.098 7.430 5.046 1.292 1.110 1.122 94.314 5.584 0.871 1.222 0.879 0.497 S33 56.122 5.352 7.029 2.854 0.739 0.561 0.474 73.131 12.837 2.978 2.015 0.584 0.334 S34 46.953 9.853 2.319 0.851 0.379 0.180 0.234 60.769 4.819 1.097 0.595 0.212 0.916 S35 56.624 15.340 0.623 1.180 5.596 1.505 0.401 81.270 6.752 1.142 0.122 0.227 0.800 S36 53.501 16.804 2.984 0.833 0.342 0.304 0.133 74.900 9.505 1.366 1.598 0.262 0.835 S37 47.872 9.927 3.013 0.885 0.564 0.353 0.141 62.754 7.241 1.305 1.148 0.379 1.002 S38 52.420 13.997 2.335 1.375 1.098 0.627 0.406 72.258 7.054 1.036 0.759 0.206 1.267 S39 50.352 13.880 5.154 0.288 0.453 0.351 0.197 70.675 6.587 0.882 1.036 1.001 0.575 S40 46.717 12.988 6.433 3.398 0.916 0.621 1.494 72.567 9.233 1.305 0.957 1.058 0.576 Average 52.470 13.209 4.399 1.802 0.734 0.428 0.383 73.425 8.006 1.191 1.082 0.607 0.756
a The sum of 7 iridoids.
