Synthesis, Characterization and Copolymerization of N-(phenylamino)maleimide with MMA

Hiran, B. L.; Paliwal, S. N.; Choudhary, Jyoti; Choudhary, P. R.

doi:https://doi.org/10.1155/2007/234768

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Volume 4 | Article ID 234768 | https://doi.org/10.1155/2007/234768

Synthesis, Characterization and Copolymerization of N-(phenylamino)maleimide with MMA

B. L. Hiran,¹S. N. Paliwal,¹Jyoti Choudhary,¹and P. R. Choudhary¹

Received23 Nov 2006

Accepted22 Dec 2006

Abstract

The free radical copolymerization of N-(phenylamino)maleimide (N-PAMI) was carried. The copolymerization with methyl methacrylate (MMA) was performed at 65°C with AIBN as the initiator in THF solvent. Resulting copolymer was characterized by density measurement, intrinsic viscosity, solubility, FT-IR & ¹H NMR spectroscopy. Effect of the solvent and time on copolymer yield was also investigated. The molecular weight of copolymer was determined by gel permeation chromatography (GPC). The thermal stability of copolymer was determined by Thermogravimetric analysis (TGA).

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Copyright © 2007 Hindawi Publishing Corporation. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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