PDF
Open Access
Synthesis, Characterizations and Investigation of Electrochemical Behaviours of 4-[(2-Hydroxyphenylimino)methyl]benzene-1,3-diol
Aysen D. Mulazimoglu,1 Ibrahim Ender Mulazimoglu
,1 and Bedrettin Mercimek11Selcuk University, Department of Chemistry, 42099, Konya, Turkey
Abstract
This Schiff base ligand, 4-[(2-hydroxyphenylimino) methyl]benzene-1,3-diol (HIBD) was synthesized by reaction of 2-aminophenol and 2,4-dihydroxybenzaldehyde. The ligand was characterized by elemental analysis, FT-IR and 1H-NMR. Electrochemical behaviors were investigated on the glassy carbon electrode (GC) surface with cyclic voltammetry (CV). The modification of HIBD on the GC was performed in +0.3 V and +2,8 V potential range using 100 mV s-1 scanning rate having 5 cycle. For the characterization of the modified surfaces 1 mM ferrocene redox probe in 0,1 M tetrabutylammonium tetrafluoroborate (TBATFB) and 1 mM ferricyanide redox probe in 0.1 M H2SO4 were used.
Copyright
Copyright © 2009 Hindawi Publishing Corporation. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
