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E-Journal of Chemistry
Volume 6, Issue 4, Pages 1247-1252
http://dx.doi.org/10.1155/2009/964534

Synthesis, Characterization and Antimicrobial Activity of Metal Chelates of 5-(4-N, N-Diethylamino sulfonyl phenyl azo)-8-hydorxy quinoline

A. U. Patel

Shri M & N. Virani Science College, “Yogidham” Kalawad Road, Rajkot, Gujarat, India

Received 31 December 2008; Accepted 25 February 2009

Copyright © 2009 Hindawi Publishing Corporation. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Abstract

4-N,N-Diethylamino sulfonyl phenyl amine was synthesized by diazotization and coupled with 8-hydroxyquinoline. The resultant 5-(4-N,N-diethylamino sulfonyl phenyl azo)-8-hydorxy quinoline (DSAQ) was characterized by elemental analysis and spectral studies. The transition metal chelates viz. Cu2+, Ni2+, Co2+, Mn2+ and Zn2+of DSAQ were prepared and characterized by metal-ligand (M:L) ratio. IR and reflectance spectroscopy and magnetic properties. The anti fungal activity of DSAQ and its metal chelates was screened against various fungi. The results show that all these samples are good antifungal agents.