Synthesis, Crystal Structure and Thermal Properties of Lead(II) Complex with Bathophenanthroline and Benzoyltrifluoroacetonate Ligands

Table 2

Selected bond lengths (Å) and angles (^°) for (1).

Pb-N1	2.779 (9)	Pb-O1	2.482 (8)
Pb-N1^i	2.779 (9)	Pb-O1^i	2.482 (8)
Pb-N2	2.871 (10)	Pb-O2	2.506 (8)
Pb-N2^i	2.871 (10)	Pb-O2^i	2.506 (8)
O1-Pb1-O1^i	91.8 (4)	O2^i-Pb1-N1	130.2 (3)
O1-Pb1-O2	71.1 (3)	N1-Pb1-N1^i	113.3 (4)
O1^i-Pb1-O2	75.8 (3)	O1-Pb1-N2^i	153.5 (3)
O1^i-Pb1-N1	84.4 (3)	O1^i-Pb1-N2^i	99.2 (3)
O2-Pb1-N2^i	135.0 (3)	N1-Pb1-N2^i	56.3 (3)
O2-Pb1-O2^i	131.7 (4)	N1^i-Pb1-N2^i	73.9 (3)
O1-Pb1-N1	149.6 (3)	O2-Pb1-N2	85.0 (3)
O2-Pb1-N1	78.7 (3)	N2^i-Pb1-N2	81.5 (4)

i: −x, y, 1/2− z.