Research Article
Synthesis, Crystal Structure and Thermal Properties of Lead(II) Complex with Bathophenanthroline and Benzoyltrifluoroacetonate Ligands
Table 3
Inter- and intramolecular interactions for 1.
| | A⋯H–B | A⋯H/Å | A⋯B/Å | A⋯H–B/° | | 1 | | | | | O1⋯H28-C28 (−x, −y, 1−z) | 2.725 | 3.360 (2) | 146.86 | | F3⋯H19-C19 (x, −y, −1/2 + z) | 2.707 | 3.308 (2) | 123.10 | | F2⋯F2(1 − x, y,1/2 − z) | — | 2.868 | — | | π⋯ π (inter, slipped face-to-face between bp ligands) | — | 3.496 | — | | π⋯ π (slipped edge-to-adge between aromatic rings of btfa-) | — | 3.507 | — | | π⋯ π (intra, slipped face-to-face between bp ligands) | — | 3.586 | — |
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