Solid-State Synthesis, Characterization, and Biological Activity of the Bioinorganic Complex of Aspartic Acid and Arsenic Triiodide

Table 1

The experimental data and the calculated results for powder X-ray diffraction pattern of title complex (monoclinic system: 𝑎=1.0019 nm, 𝑏=1.5118 nm, 𝑐=2.1971 nm, 𝛽=100.28^∘).

No.	ℎ	𝑘	𝑙	𝑑exp/nm	𝑑cal/nm	𝐼/𝐼0
1	0	2	1	0.7132	0.7135	6.9
2	1	2	0	0.6011	0.5999	0.8
3	1	0	3	0.5374	0.5378	7.9
4	0	1	4	0.5092	0.5089	2.5
5	−1	1	5	0.4088	0.4090	23.0
6	−2	1	4	0.3893	0.3882	7.2
7	1	2	4	0.3820	0.3815	3.0
8	0	2	5	0.3744	0.3753	7.3
9	0	4	2	0.3570	0.3568	85.3
10	−2	3	2	0.3481	0.3484	5.4
11	2	3	1	0.3398	0.3409	6.4
12	−3	1	0	0.3211	0.3211	100.0
13	3	0	1	0.3159	0.3166	15.0
14	1	4	4	0.2868	0.2872	12.5
15	−3	3	2	0.2772	0.2768	1.1
16	−2	5	1	0.2591	0.2588	4.1
17	2	2	6	0.2533	0.2534	22.4
18	−1	1	9	0.2407	0.2405	6.2
19	3	4	2	0.2351	0.2349	2.1
20	−2	4	7	0.2277	0.2279	3.3
21	−4	3	3	0.2217	0.2219	1.4
22	−2	5	7	0.2077	0.2076	36.5
23	3	0	7	0.2072	0.2073	1.0
24	−3	6	3	0.1983	0.1983	16.8
25	−5	2	5	0.1868	0.1869	1.3
26	−4	5	6	0.1796	0.1794	20.8
27	3	2	9	0.1745	0.1744	11.0
28	−5	3	7	0.1707	0.1708	1.2
29	−6	0	0	0.1644	0.1643	1.4
30	−6	1	6	0.1598	0.1598	4.2
31	2	8	8	0.1435	0.1436	3.6
32	−6	6	6	0.1354	0.1355	3.9
33	2	9	8	0.1337	0.1337	5.6
34	5	7	5	0.1327	0.1328	2.9
35	5	6	8	0.1272	0.1271	1.9
36	7	6	2	0.1201	0.1201	0.8