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Journal of Chemistry
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2013
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Article
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Tab 3
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Research Article
Acetylation of Phenols, Anilines, and Thiols Using Silica Sulfuric Acid under Solvent-Free Conditions
Table 3
Acylation of 2-naphthol with Ac
2
O by SSA in solvent-free condition at room temperature.
Entry
2-Naphthol : Ac
2
O (mole ratio)
Yield %
1
1.0 : 1.0
40
2
1.0 : 1.2
50
3
1.0 : 1.5
70
4
1.0 : 1.7
83
5
1.0 : 2.0
90