Research Article
Synthesis and Single Crystal X-Ray Structure of New (2E)-2-[3-(1H-Imidazol-1-yl)-1-phenylpropylidene]-N-phenylhydrazinecarboxamide
Table 1
Crystallographic data and refinement information.
| | Empirical formula | C19H19N5O | | Formula weight | 333.39 | | Temperature (K) | 296 | | Crystal system | Monoclinic | | Space group | | | Cu Kα radiation, | 1.54178 Å | | (Å) | 5.8093 (2) | | (Å) | 20.5575 (6) | | (Å) | 14.0355 (5) | | (°) | 90.00 | | (°) | 97.365 (2) | | (°) | 90.00 | | (Å3) | 1662.36 (10) | | 4 | | (000) | 704 | | Theta range for data collection (°) | 3.8–62.9 | | (mm−1) | 0.70 | | Density (calc.) (g/cm3) | 1.332 | | Crystal shape and color | Needle, colorless | | Crystal size (mm3) | 0.42 × 0.11 × 0.09 | |
−4.6/−24.25/−16.16 | | Measured reflections | 10883 | | Independent reflections | 3009 [ = 0.074] | | Reflections with > | 1536 | | Goodness-of-fit on | 0.97 | | 0.075 | | 0.252 | | (e Å−3) | 0.35 | | (e Å−3) | −0.28 |
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