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Journal of Chemistry
/
2013
/
Article
/
Tab 1
/
Research Article
An Efficient Green Procedure for Synthesis of Some Fluorinated Curcumin Analogues Catalyzed by Calcium Oxide under Microwave Irradiation and Its Antibacterial Evaluation
Table 1
Physical and analytical data of curcumin analogues
1
–
5
.
Compound
Time (sec)
Yield (%)
Melting point (
C)
Elemental analysis (%)
(M–H)
+•
, molecular formula
C found (calculated)
H found (calculated)
1
90
82
219–221
72.70 (73.07)
4.48 (4.52)
311, C
19
H
14
F
2
O
2
2
60
88
250–253
65.30 (65.52)
3.42 (3.47)
347, C
19
H
12
F
4
O
2
3
120
92
260–264
65.30 (65.52)
3.42 (3.47)
347, C
19
H
12
F
4
O
2
4
120
94
253–255
65.30 (65.52)
3.42 (3.47)
347, C
19
H
12
F
4
O
2
5
90
85
265–267
65.30 (65.52)
3.42 (3.47)
347, C
19
H
12
F
4
O
2