Research Article
Synthesis and Crystal Structure of N-Dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine
Table 3
Atomic coordinates (×104) and equivalent isotropic displacement parameter (×103) for nonhydrogen atoms.
| | Atom | | | | (eq) |
| | Cl(1) | −645(1) | −526(1) | −3480(1) | 54(1) | | Cl(2) | 2826(2) | −3055(1) | 2329(1) | 64(1) | | Cl(3) | 5737(2) | −2142(1) | 4698(1) | 78(1) | | O(1) | −3560(4) | −841(1) | 958(2) | 47(1) | | O(2) | 898(4) | −2134(1) | 13(2) | 53(1) | | N(1) | 95(3) | −1573(1) | 1441(2) | 31(1) | | C(1) | −3748(5) | −352(1) | −1179(3) | 40(1) | | C(2) | −3095(4) | −263(1) | −2227(3) | 38(1) | | C(3) | −1416(4) | −620(1) | −2102(3) | 35(1) | | C(4) | −352(4) | −1056(1) | −932(3) | 33(1) | | C(5) | −1032(4) | −1149(1) | 128(2) | 30(1) | | C(6) | −2780(4) | −793(1) | −26(3) | 35(1) | | C(7) | −2769(5) | −1322(1) | 2000(3) | 42(1) | | C(8) | 28(5) | −1468(1) | 2915(3) | 36(1) | | C(9) | 1973(5) | −1033(1) | 4209(3) | 48(1) | | C(10) | 1082(4) | −2026(1) | 1307(3) | 34(1) | | C(11) | 2579(4) | −2413(1) | 2954(3) | 37(1) |
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