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Journal of Chemistry
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2017
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Article
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Tab 2
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Research Article
An Efficient Synthesis of Milnacipran Hydrochloride via Reductive Amination of Aldehyde
Table 2
Reagent mole equivalent optimization table.
Entry
DMP
Solvent
Yield%
1
0.8
DCM
50
2
0.9
DCM
70
3
1.0
DCM
83
4
1.1
MDC
95
b: Dess-Martin periodinane reagent.