Research Article

Solvent-Free Henry and Michael Reactions with Nitroalkanes Promoted by Potassium Carbonate as a Versatile Heterogeneous Catalyst

Table 1

Optimization of nitroaldol reaction using K2CO3.

Entry
RR1R2Mol (%)
catalyst
Temperature (°C)Time (h)Yield of 3
(%)

1PhCH3H10252435
2CH3CH3H30252454
3CH3CH3H1060448
4CH3CH2CH2CH3H30252458
5CH3CH2CH2CH3H10604 68

Yield of pure isolated products.