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Journal of Chemistry
/
2017
/
Article
/
Tab 1
/
Research Article
Synthesis of Isoxazolopyridines and Spirooxindoles under Ultrasonic Irradiation and Evaluation of Their Antioxidant Activity
Table 1
Optimization of (±)-CSA catalyst loading in the synthesis of compound
4a
.
(±)-CSA (mol%)
Temperature (°C)
Conditions
Time (min)
Yield
—
40
US
300
35
5
40
US
180
52
5
70
US
120
58
10
70
US
120
65
15
70
US
120
71
20
70
US
120
72
20
78
Δ/reflux
360
51
yield.