Development of a Methodology for the Determination of Pesticide Residues in Cajá-Manga Pulp (Spondias dulcis L.) Using Solid-Liquid Extraction with Low-Temperature Partitioning

Table 3

Accuracy (% recoveries) and precision (repeatability and within-laboratory reproducibility) of the SLE-LTP method developed ().

Pesticides	Repeatability						Within-lab reproducibility
	2 × LOQ		3 × LOQ		4 × LOQ		4 × LOQ
	Recovery (%)	RSDr (%)	Recovery (%)	RSDr (%)	Recovery (%)	RSDr (%)	Recovery (%)	RSDwR (%)
Chlorpyrifos	96	22	95	13	89	6	88	2
Thiabendazole	188	14	129	7	117	6	111	5
Carboxin	69	26	78	8	82	11	76	7
Difenoconazole	80	13	90	4	109	9	102	6

= Outlier value. A value above the acceptable range of recoveries for compounds in complex matrices.