Synthesis and Crystalline Structure of Zinc Complexes with Antihypertensive Drug Lisinopril

Table 2

Crystal data for LISZn2 compound.

Compound	LISZn2
Chemical formula	C84H148N12O36Zn4
Formula weight (g·mol^−1)	2163.61
Crystal system	Trigonal
Space group	P32
a (Å)	27.4727(7)
b (Å)	27.4727(7)
c (Å)	11.4613(3)
α (°)	90
β (°)	90
γ (°)	120
Volume (Å^3)	7491.5(4)
Z	3
Temperature (K)	120.0(1)
dcalc. (g·cm^−3)	1.439
μ (KαCu) (mm^−1)	1.835
Crystal size (mm)	0.12 × 0.11 × 0.09
Radiation	λ = 1.5418 Å (KαCu)
θ limits (°)	3.1980–72.5730
Refl. measured/independent	24164/15047
Refl. observed [Fobs > 4σ(Fobs)]	11695
Parameters	1189
Flack parameter	0.023(11)
Rint	0.0356
R [Fobs > 4σ(Fobs)]	0.0609
R indices for all data	0.0777
wR [Fobs > 4σ(Fobs)]	0.1635
Goodness-of-fit (GOF)	1.06
Weighting scheme	W = 1/[σ^2(Fo^2) + (0.1137P)^2 + 0.0000P]; Where P = (Fo^2 + 2Fc^2)/3
(Δρ)min, (Δρ)max (e·Å^−3)	−0.71, 1.55