Research Article

Basic Ionic Liquid as Catalyst in Synthesis of Dimethyl 4-(2-(2,6-Bis(methoxycarbonyl)pyridine-4-yl)vinyl)pyridine-2,6-dicarboxylate

Table 2

Effects of reaction temperature on the reaction.

EntryTemperature°CYield (%)

3042
4064
5078
6083
7081
8082
9079
10071

Reaction conditions: (25 mmol), tetrahydrofuran 60 ml, [bmim]OH (2.5 mmol), CH3OH (40 ml), 40 min. yield.