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Journal of Chemistry
/
2019
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Article
/
Tab 2
/
Research Article
Synthesis, Characterization, and Antibacterial Activities of 1H-Imidazo [5, 6-f] [1,10] Phenanthroline-2(3H)-Thione and Its Ni(II) and Cu(II) Complexes
Table 2
1
H-NMR,
13
C NMR, and DEPT 135 of the ligand as depicted in Figure
1
.
Proton (assigned)
1
H NMR
δ
(ppm)
Carbon (assigned)
13
C NMR
δ
(ppm)
Group (assigned)
DEPT
δ
(ppm)
H(2), H(9)
8.72
C(2), C(9)
150.7
C-H
150.7
H(4), H(7)
8.25
C(5), C(6)
147.0
C
—
H(3), H(8)
7.55
C(4), C(7)
136.6
C-H
136.6
H(16), H(17)
9.55
C(11), C(13)
132.5
C
—
C(3), C(8)
125.1
C-H
125.1
C(12), C(14)
85.8
C
—
C(15)
182.2
—