Research Article

Organocatalytic Cascade Reaction of Aliphatic Enals and Benzoylnitromethane: Synthesis of Enantioenriched Tetrasubstituted Cyclohexene Carbaldehyde

Table 2

Correlations for compound Michael adduct 3c in the COSY spectrum.

Protonδ (ppm)Correlation

10.922 (1.44–1.31)
21.44–1.311 (0.92), 2 (1.44–1.31), 4 (2.76–2.68)
32.69–2.544 (2.71), 9 (9.77)
42.76–2.682 (1.44–1.31), 3 (2.69–2.54), 5 (4.44)
54.444 (2.76–2.68)
67.50–7.457 (7.63–7.59), 8 (8.13–8.10)
77.63–7.596 (7.50–7.45)
88.13–8.106 (7.50–7.45)
99.973 (2.69–2.54)