Research Article
Organocatalytic Cascade Reaction of Aliphatic Enals and Benzoylnitromethane: Synthesis of Enantioenriched Tetrasubstituted Cyclohexene Carbaldehyde
Table 2
Correlations for compound Michael adduct 3c in the COSY spectrum.
| Proton | δ (ppm) | Correlation |
| 1 | 0.92 | 2 (1.44–1.31) | 2 | 1.44–1.31 | 1 (0.92), 2 (1.44–1.31), 4 (2.76–2.68) | 3 | 2.69–2.54 | 4 (2.71), 9 (9.77) | 4 | 2.76–2.68 | 2 (1.44–1.31), 3 (2.69–2.54), 5 (4.44) | 5 | 4.44 | 4 (2.76–2.68) | 6 | 7.50–7.45 | 7 (7.63–7.59), 8 (8.13–8.10) | 7 | 7.63–7.59 | 6 (7.50–7.45) | 8 | 8.13–8.10 | 6 (7.50–7.45) | 9 | 9.97 | 3 (2.69–2.54) |
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