Microstructural Study of ZnO Nanostructures by Rietveld Analysis

Table 2

Results of Rietveld refinement.

Sample	Rp	Rwp	GofF	Lattice parameters			Preferred orientation		Size parameters		B overall (Å^2)	𝑍 Oxygen
				a (Å)	c (Å)	c/a	G1 (101)	Vol. oriented %	Y	S (Z)
Z1	15.5	12.2	0.8	3.247	5.203	1.602	0.857	8.9	0.025	0.471	1.64	0.374
Z2	17.6	12.8	0.8	3.251	5.209	1.602	0.828	10.9	0.021	0.465	1.43	0.375
Z3	21.2	15.0	0.9	3.250	5.206	1.602	0.830	10.5	0.026	0.695	2.09	0.370
Z4	50.7	28.2	0.8	3.254	5.212	1.602	0.730	18.0	0.369	-5.20	2.37	0.367
Z5	17.0	12.6	0.9	3.252	5.211	1.602	0.821	11.3	0.038	0.137	1.04	0.374
Z6	16.6	12.9	0.9	3.251	5.209	1.602	0.816	11.7	0.041	0.116	1.47	0.375
Z7	12.6	10.7	1.0	3.252	5.212	1.602	0.861	8.6	0.031	0.414	0.65	0.378
Z8	14.3	12.1	0.9	3.251	5.212	1.603	0.922	4.7	0.025	0.576	1.11	0.370
Z9	35.0	22.6	0.9	3.249	5.205	1.602	0.799	12.9	0.045	0.397	2.30	0.373
Z10	27.9	19.1	0.9	3.250	5.208	1.602	0.801	12.7	0.038	0.217	1.66	0.369
Z11	23.6	17.4	1.2	3.251	5.210	1.602	0.778	14.4	0.036	0.152	1.56	0.376
Z12	37.5	23.8	0.8	3.245	5.198	1.602	0.762	15.5	0.023	0.625	2.70	0.364
Z13	29.1	20.0	0.9	3.251	5.208	1.602	0.899	6.1	0.019	0.765	2.30	0.372
Z14	32.8	21.5	0.9	3.243	5.196	1.602	0.809	12.2	0.020	0.543	2.03	0.372