Research Article
Microstructural Study of ZnO Nanostructures by Rietveld Analysis
Table 4
Crystallite domains and dimension ratio obtained by GIXRD and SEM (units in nanometers). *Poor quality in diffraction data.
| Sample | GIXRD | SEM | Crystallite domains, | L | D | L/D | Normal to (002) planes | Normal to (100) planes | / |
| Z1 | 228 | 112 | 2.0 | 1341 ± 343 | 467 ± 109 | 2.9 | Z2 | 264 | 119 | 2.2 | 1706 ± 317 | 422 ± 170 | 4.0 | Z3 | 205 | 86 | 2.4 | 2221 ± 533 | 443 ± 123 | 5.0 | Z4* | 16* | 73* | 0.2* | 1934 ± 375 | 369 ± 97 | 5.2 | Z5 | 151 | 125 | 1.2 | 1283 ± 225 | 221 ± 58 | 5.8 | Z6 | 136 | 118 | 1.2 | 1278 ± 233 | 238 ± 48 | 5.4 | Z7 | 184 | 105 | 1.7 | 821 ± 175 | 115 ± 30 | 7.1 | Z8 | 222 | 97 | 2.3 | 1280 ± 270 | 173 ± 45 | 7.4 | Z9 | 140 | 92 | 1.5 | 1889 ± 329 | 444 ± 102 | 4.3 | Z10 | 148 | 112 | 1.3 | 2109 ± 484 | 498 ± 73 | 4.2 | Z11 | 154 | 126 | 1.2 | 1669 ± 377 | 599 ± 189 | 2.8 | Z12 | 242 | 98 | 2.5 | 1762 ± 445 | 470 ± 126 | 3.7 | Z13 | 295 | 91 | 3.2 | 1425 ± 420 | 331 ± 149 | 4.3 | Z14 | 270 | 111 | 2.4 | 1803 ± 771 | 437 ± 182 | 4.1 |
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