Preparation, Properties, and Self-Assembly Behavior of PTFE-Based Core-Shell Nanospheres

Table 4

Sample composition derived from TGA and DSC, glass transition temperature, diameter estimated, PCS Size, SEM size, and uniformity ratio of the various samples.

Sample	% PTFE Theorical (W/W)	% PTFE (TGA)	% PTFE (DSC)	d estimated (nm)	d PCS (nm)	d SEM (nm)	Uniformity Ratio U
MDS1	0.25	0.21	0.11	383	417	380	1.003
MDS2	0.50	0.47	0.33	304	309	301	1.004
MDS3	1.00	0.85	0.67	241	245	237	1.005
MDS4	3.00	2.91	2.08	167	166	163	1.007
MDS5*	5.20	5.20	4.30	138	139	133	1.012
MDS6	9.00	8.70	7.67	114	115	111	1.028
MDS7*	9.80	6.70	7.9	111	113	107	1.030
MDS8*	17.90	19.4	16.8	89	92	84	1.050
MDS9*	24.50	22.7	22.7	80	89	75	1.100
D60GS1	12.5	12.0	12.4	596	604	593	1.004
D60GS2	19.0	18.0	19.3	511	525	500	1.004

*Published in [31].