Research Article

Solvothermal Synthesis of Mn3O4 Nanoparticle/Graphene Sheet Composites and Their Supercapacitive Properties

Table 1

Synthesized conditions and electrochemical performances of Mn3O4/graphene composites prepared by hydrothermal or solvothermal routes in published literatures.

Basic synthesis informationElectrolytePotential window (V)Current loador scan rateMaximum specific capacitance (F/g)Reference

Graphene sheets + KMnO4 + H2O + ethylene glycol,
solvothermal 393 K for 4 h
1 M Na2SO4−0.3 to 0.7
(Ag/Ag Cl)
5 mV/s120 (3-electrode)[22]

GO + Mn(CH3COO2)·4H2O + ethanol + H2O,
solvothermal 453 K for 11 h
1 M Na2SO4−0.2 to 0.8
(SCE)
5 mV/s225 (3-electrode)[23]

GO + KMnO4 + H2O + hydrazine hydrate,
hydrothermal 453 K for 6 h
1 M Na2SO4−0.2 to 0.8
(SCE)
0.1 A/g171 (3-electrode)[24]

GO + Mn(CH3COO2)·4H2O + dimethyl sulfoxide
solvothermal 393 K for 24 h
1 M Na2SO4−0.2 to 0.8
(SCE)
0.1 A/g147 (3-electrode)[29]