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Journal of Nanomaterials
Volume 2015, Article ID 316057, 5 pages
Research Article

Facile Synthesis of N-Doped BiOCl Photocatalyst by an Ethylenediamine-Assisted Hydrothermal Method

1School of Pharmaceutical and Chemical Engineering, Taizhou University, Jiaojiang 318000, China
2Jiangsu Key Laboratory for Environment Functional Materials, Suzhou University of Science and Technology, Suzhou 215009, China
3School of Bioscience, Taizhou University, Taizhou, Jiaojiang 318000, China

Received 25 January 2015; Revised 13 April 2015; Accepted 21 April 2015

Academic Editor: Marinella Striccoli

Copyright © 2015 Guihua Chen et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.


A nitrogen doped BiOCl (N-BiOCl) photocatalyst was synthesized and characterized using an ethylenediamine-assisted hydrothermal method. The N-BiOCl sample demonstrated the same tetragonal crystal structure as the as-prepared pure BiOCl sample. SEM results indicated that N-BiOCl sample was self-assembled by nanoplates to provide an aggregated flower-like microstructure. Doped nitrogen was substituted for oxygen in the crystal lattice of BiOCl, causing a red shift for N-BiOCl sample compared to BiOCl sample. The N-BiOCl sample exhibited higher photocatalytic activity in the degradation of Rhodamine B under visible light than observed in BiOCl sample, and the stability of the sample was verified. Meanwhile, speculative causes for the enhancement in the photocatalytic activity of N-BiOCl sample were also proposed.