Research Article

Titanium Carbide Nanocrystals Synthesized from a Metatitanic Acid-Sucrose Precursor via a Carbothermal Reduction

Table 1

Specific surface area, specific pore volume, and average pore diameter of the (a) as-received MTA, (b) MTA heat-treated at 600°C for 1 h in air, (c) TiC synthesized from precursor T at 1500°C, and (d) TiC synthesized from precursor M at 1500°C.

Samples(a)(b) (c)(d)

Specific surface area (BET; m2/g)377.379.3894.7879.41

Average pore diameter (BJH desorption; nm)3.888.4319.7 & 2.625.0 & 2.6

Specific pore volume (BJH desorption; cm3/g)0.300.270.200.10