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Journal of Nanomaterials
Volume 2017, Article ID 5794312, 10 pages
https://doi.org/10.1155/2017/5794312
Research Article

Synthesis of Carbon Nanofibers with Maghemite via a Modified Sol-Gel Technique

1Engineering Institute, Autonomous University of Baja California, 21100 Mexicali, BC, Mexico
2Centro Nacional de Investigaciones Metalúrgicas (CENIM), CSIC, Avda. Gregorio del Amo 8, 28040 Madrid, Spain

Correspondence should be addressed to Benjamín Valdez Salas; xm.ude.cbau@lavneb

Received 11 July 2017; Accepted 31 July 2017; Published 9 November 2017

Academic Editor: Andrew R. Barron

Copyright © 2017 Nicolás Díaz Silva et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Linked References

  1. X.-L. Wang, I.-K. Oh, and J.-B. Kim, “Enhanced electromechanical performance of carbon nano-fiber reinforced sulfonated poly(styrene-b-[ethylene/butylene]-b-styrene) actuator,” Composites Science and Technology, vol. 69, no. 13, pp. 2098–2101, 2009. View at Publisher · View at Google Scholar · View at Scopus
  2. J. H. Lehman, M. Terrones, E. Mansfield, K. E. Hurst, and V. Meunier, “Evaluating the characteristics of multiwall carbon nanotubes,” Carbon, vol. 49, no. 8, pp. 2581–2602, 2011. View at Publisher · View at Google Scholar · View at Scopus
  3. M. H. Al-Saleh and U. Sundararaj, “Review of the mechanical properties of carbon nanofiber/polymer composites,” Composites Part A: Applied Science and Manufacturing, vol. 42, no. 12, pp. 2126–2142, 2011. View at Publisher · View at Google Scholar · View at Scopus
  4. E. Enríquez, J. de Frutos, J. F. Fernández, and M. A. de la Rubia, “Conductive coatings with low carbon-black content by adding carbon nanofibers,” Composites Science and Technology, vol. 93, pp. 9–16, 2014. View at Publisher · View at Google Scholar · View at Scopus
  5. S. Bal, S. S. Samal, and U. K. Mohanty, “Mechanical and microstructural analysis of carbon nanotube composites pretreated at different temperatures,” American Journal of Materials Science, vol. 1, no. 1, pp. 5–11, 2011. View at Google Scholar
  6. D. Zhou, E. V. Anoshkina, L. Chow, and G. Chai, “Synthesis of carbon nanotubes by electrochemical deposition at room temperature,” Carbon, vol. 44, no. 5, pp. 1013–1016, 2006. View at Publisher · View at Google Scholar · View at Scopus
  7. C. L. Cheung, A. Kurtz, H. Park, and C. M. Lieber, “Diameter-controlled synthesis of carbon nanotubes,” The Journal of Physical Chemistry B, vol. 106, no. 10, pp. 2429–2433, 2002. View at Publisher · View at Google Scholar · View at Scopus
  8. M. V. Reddy, G. V. Subba Rao, and B. V. R. Chowdari, “Metal oxides and oxysalts as anode materials for Li ion batteries,” Chemical Reviews, vol. 113, no. 7, pp. 5364–5457, 2013. View at Publisher · View at Google Scholar · View at Scopus
  9. Y. Wu, P. Zhu, M. V. Reddy, B. V. R. Chowdari, and S. Ramakrishna, “Maghemite nanoparticles on electrospun CNFs template as prospective lithium-ion battery anode,” ACS Applied Materials & Interfaces, vol. 6, no. 3, pp. 1951–1958, 2014. View at Publisher · View at Google Scholar · View at Scopus
  10. Y. Wu, M. V. Reddy, B. V. R. Chowdari, and S. Ramakrishna, “Long-term cycling studies on electrospun carbon nanofibers as anode material for lithium ion batteries,” ACS Applied Materials & Interfaces, vol. 5, no. 22, pp. 12175–12184, 2013. View at Publisher · View at Google Scholar · View at Scopus
  11. A. S. Hameed, M. V. Reddy, B. V. R. Chowdari, and J. J. Vittal, “Preparation of rGO-wrapped magnetite nanocomposites and their energy storage properties,” RSC Advances, vol. 4, no. 109, pp. 64142–64150, 2014. View at Publisher · View at Google Scholar · View at Scopus
  12. S. Petnikota, H. Maseed, V. V. S. S. Srikanth et al., “Experimental Elucidation of a Graphenothermal Reduction Mechanism of Fe2O3: An Enhanced Anodic Behavior of an Exfoliated Reduced Graphene Oxide/Fe3O4 Composite in Li-Ion Batteries,” The Journal of Physical Chemistry C, vol. 121, no. 7, pp. 3778–3789, 2017. View at Publisher · View at Google Scholar · View at Scopus
  13. M. V. Reddy, C. T. Cherian, K. Ramanathan et al., “Molten synthesis of ZnO.Fe3O4 and Fe2O3 and its electrochemical performance,” Electrochimica Acta, vol. 118, pp. 75–80, 2014. View at Publisher · View at Google Scholar · View at Scopus
  14. C. T. Cherian, J. Sundaramurthy, M. Kalaivani et al., “Electrospun α-Fe2O3 nanorods as a stable, high capacity anode material for Li-ion batteries,” Journal of Materials Chemistry, vol. 22, no. 24, pp. 12198–12204, 2012. View at Publisher · View at Google Scholar · View at Scopus
  15. M. V. Reddy, T. Yu, C.-H. Sow et al., “α-Fe2O3 nanoflakes as an anode material for li-ion batteries,” Advanced Functional Materials, vol. 17, no. 15, pp. 2792–2799, 2007. View at Publisher · View at Google Scholar · View at Scopus
  16. J. Jia, X. Sun, X. Lin, X. Shen, Y.-W. Mai, and J.-K. Kim, “Exceptional electrical conductivity and fracture resistance of 3D interconnected graphene foam/epoxy composites,” ACS Nano, vol. 8, no. 6, pp. 5774–5783, 2014. View at Publisher · View at Google Scholar · View at Scopus
  17. C. Lake and P. Lake, “Carbon nanofiber multifunctional mat,” in Nanotube Superfiber Materials Changing Engineering Design, M. Schulz, V. Shanov, and Z. Yin, Eds., pp. 313–331, William Andrew Applied Science Publishers, Waltham, Massachusetts, Mass, USA, 1st edition, 2014. View at Google Scholar
  18. I. Kang, Y. Y. Heung, J. H. Kim et al., “Introduction to carbon nanotube and nanofiber smart materials,” Composites Part B: Engineering, vol. 37, no. 6, pp. 382–394, 2006. View at Publisher · View at Google Scholar · View at Scopus
  19. B. M. Tyson, R. K. Abu Al-Rub, A. Yazdanbakhsh, and Z. Grasley, “A quantitative method for analyzing the dispersion and agglomeration of nano-particles in composite materials,” Composites Part B: Engineering, vol. 42, no. 6, pp. 1395–1403, 2011. View at Publisher · View at Google Scholar · View at Scopus
  20. K. A. Wepasnick, B. A. Smith, J. L. Bitter, and D. H. Fairbrother, “Chemical and structural characterization of carbon nanotube surfaces,” Analytical and Bioanalytical Chemistry, vol. 396, no. 3, pp. 1003–1014, 2010. View at Publisher · View at Google Scholar · View at Scopus
  21. S. Bal, “Experimental study of mechanical and electrical properties of carbon nanofiber/epoxy composites,” Materials and Corrosion, vol. 31, no. 5, pp. 2406–2413, 2010. View at Publisher · View at Google Scholar · View at Scopus
  22. C.-S. Lim, A. J. Rodriguez, M. E. Guzman, J. D. Schaefer, and B. Minaie, “Processing and properties of polymer composites containing aligned functionalized carbon nanofibers,” Carbon, vol. 49, no. 6, pp. 1873–1883, 2011. View at Publisher · View at Google Scholar · View at Scopus
  23. I. Kim and R. Tannenbaum, “Magnetic carbon nanotubes: synthesis, characterization, and anisotropic electrical properties,” in Electronic Properties of Carbon Nanotubes, pp. 33–55, InTech, Rijeka, Croatia, 2011. View at Google Scholar
  24. I. T. Kim, G. A. Nunnery, K. Jacob, J. Schwartz, X. Liu, and R. Tannenbaum, “Synthesis, characterization, and alignment of magnetic carbon nanotubes tethered with maghemite nanoparticles,” The Journal of Physical Chemistry C, vol. 114, no. 15, pp. 6944–6951, 2010. View at Publisher · View at Google Scholar · View at Scopus
  25. I. T. Kim, A. Tannenbaum, and R. Tannenbaum, “Anisotropic conductivity of magnetic carbon nanotubes embedded in epoxy matrices,” Carbon, vol. 49, no. 1, pp. 54–61, 2011. View at Publisher · View at Google Scholar · View at Scopus
  26. S. Wu, R. B. Ladani, J. Zhang et al., “Epoxy nanocomposites containing magnetite-carbon nanofibers aligned using a weak magnetic field,” Polymer Journal, vol. 68, pp. 25–34, 2015. View at Publisher · View at Google Scholar
  27. H. Varela-Rizo, S. Bittolo-Bon, I. Rodriguez-Pastor, L. Valentini, and I. Martin-Gullon, “Processing and functionalization effect in CNF/PMMA nanocomposites,” Composites Part A: Applied Science and Manufacturing, vol. 43, no. 4, pp. 711–721, 2012. View at Publisher · View at Google Scholar · View at Scopus
  28. Z. Zhao, Z. Yang, Y. Hu, J. Li, and X. Fan, “Multiple functionalization of multi-walled carbon nanotubes with carboxyl and amino groups,” Applied Surface Science, vol. 276, pp. 476–481, 2013. View at Publisher · View at Google Scholar · View at Scopus
  29. M. I. Barrena, J. M. Gómez De Salazar, A. Soria, and R. Cañas, “Improved of the wear resistance of carbon nanofiber/epoxy nanocomposite by a surface functionalization of the reinforcement,” Applied Surface Science, vol. 289, pp. 124–128, 2014. View at Publisher · View at Google Scholar · View at Scopus
  30. A. G. Osorio, I. C. L. Silveira, V. L. Bueno, and C. P. Bergmann, “H2SO4/HNO3/HCl-Functionalization and its effect on dispersion of carbon nanotubes in aqueous media,” Applied Surface Science, vol. 255, no. 5, pp. 2485–2489, 2008. View at Publisher · View at Google Scholar · View at Scopus
  31. J. Zhang, T. Lin, and X. Wang, “Carbon and polymer nanofiber reinforcements in polymer matrix composites: processing and applications,” in Functional nanofibers and their applications, pp. 55–70, Woodhead, Philadelphia, Pennsylvania, Pa, USA, 2012. View at Google Scholar
  32. S. G. Prolongo, M. Burón, M. R. Gude, R. Chaos-Morán, M. Campo, and A. Ureña, “Effects of dispersion techniques of carbon nanofibers on the thermo-physical properties of epoxy nanocomposites,” Composites Science and Technology, vol. 68, no. 13, pp. 2722–2730, 2008. View at Publisher · View at Google Scholar · View at Scopus
  33. Y. Harel, S. Azoubel, S. Magdassi, and J.-P. Lellouche, “A dispersability study on poly(thiophen-3-yl-acetic acid) and PEDOT multi-walled carbon nanotube composites using an analytical centrifuge,” Journal of Colloid and Interface Science, vol. 390, no. 1, pp. 62–69, 2013. View at Publisher · View at Google Scholar · View at Scopus
  34. K. Safarova, A. Dvorak, R. Kubinek, M. Vujtek, and A. Rek, “Usage of AFM, SEM and TEM for the research of carbon nanotubes,” in Modern Research and Educational Topics in Microscopy, vol. 5, pp. 513–519, Formatex, Bandajoz, Spain, 2007. View at Google Scholar
  35. G. Woehrle, J. Hutchinson, S. Ozkar, and R. Finke, “Analysis of nanoparticle transmission electron microscopy data using a public- domain image-processing program, image,” Turkish Journal of Chemistry, vol. 30, pp. 1–13, 2006. View at Google Scholar
  36. F. Solá, Z. H. Xia, M. Lebrón-Colón, and M. A. Meador, “Transmission electron microscopy of single wall carbon nanotube/polymer nanocomposites: a first-principles study,” Physica Status Solidi - Rapid Research Letters, vol. 6, no. 8, pp. 349–351, 2012. View at Publisher · View at Google Scholar · View at Scopus
  37. H. Cui, Y. Liu, and W. Ren, “Structure switch between α-Fe2O3, γ-Fe2O3 and Fe3O4 during the large scale and low temperature sol-gel synthesis of nearly monodispersed iron oxide nanoparticles,” Advanced Powder Technology, vol. 24, no. 1, pp. 93–97, 2013. View at Publisher · View at Google Scholar · View at Scopus
  38. W. Wu, X. H. Xiao, S. F. Zhang et al., “Synthesis and magnetic properties of maghemite (γ-Fe2O3) short-nanotubes,” Nanoscale Research Letters, vol. 5, no. 9, pp. 1474–1479, 2010. View at Publisher · View at Google Scholar · View at Scopus
  39. Y. Lu, Y. Yin, B. T. Mayers, and Y. Xia, “Modifying the surface properties of superparamagnetic iron oxide nanoparticles through a sol-gel approach,” Nano Letters, vol. 2, no. 3, pp. 183–186, 2002. View at Publisher · View at Google Scholar · View at Scopus
  40. D. Rosenthal, M. Ruta, R. Schlögl, and L. Kiwi-Minsker, “Combined XPS and TPD study of oxygen-functionalized carbon nanofibers grown on sintered metal fibers,” Carbon, vol. 48, no. 6, pp. 1835–1843, 2010. View at Publisher · View at Google Scholar · View at Scopus
  41. T.-C. Lin, G. Seshadri, and J. A. Kelber, “A consistent method for quantitative XPS peak analysis of thin oxide films on clean polycrystalline iron surfaces,” Applied Surface Science, vol. 119, no. 1-2, pp. 83–92, 1997. View at Publisher · View at Google Scholar · View at Scopus
  42. T. Yamashita and P. Hayes, “Analysis of XPS spectra of Fe2+ and Fe3+ ions in oxide materials,” Applied Surface Science, vol. 254, no. 8, pp. 2441–2449, 2008. View at Publisher · View at Google Scholar
  43. T. Fujii, F. M. F. De Groot, G. A. Sawatzky, F. C. Voogt, T. Hibma, and K. Okada, “In situ XPS analysis of various iron oxide films grown by NO2-assisted molecular-beam epitaxy,” Physical Review B: Condensed Matter and Materials Physics, vol. 59, no. 4, pp. 3195–3202, 1999. View at Publisher · View at Google Scholar · View at Scopus
  44. M. V. Reddy, N. Sharma, S. Adams, R. P. Rao, V. K. Peterson, and B. V. R. Chowdari, “Evaluation of undoped and M-doped TiO2, where M = Sn, Fe, Ni/Nb, Zr, V, and Mn, for lithium-ion battery applications prepared by the molten-salt method,” RSC Advances, vol. 5, no. 37, pp. 29535–29544, 2015. View at Publisher · View at Google Scholar · View at Scopus
  45. J. I. Paredes, M. Burghard, A. Martínez-Alonso, and J. M. D. Tascón, “Graphitization of carbon nanofibers: visualizing the structural evolution on the nanometer and atomic scales by scanning tunneling microscopy,” Applied Physics A: Materials Science & Processing, vol. 80, no. 4, pp. 675–682, 2005. View at Publisher · View at Google Scholar · View at Scopus
  46. X. Du, H.-Y. Liu, G. Cai, Y.-W. Mai, and A. Baji, “Use of facile mechanochemical method to functionalize carbon nanofibers with nanostructured polyaniline and their electrochemical capacitance,” Nanoscale Research Letters, vol. 7, article no. 111, pp. 1–10, 2012. View at Publisher · View at Google Scholar · View at Scopus
  47. W. Kim, C.-Y. Suh, S.-W. Cho et al., “A new method for the identification and quantification of magnetite-maghemite mixture using conventional X-ray diffraction technique,” Talanta, vol. 94, pp. 348–352, 2012. View at Publisher · View at Google Scholar · View at Scopus
  48. Y. Wang, S. Serrano, and J. J. Santiago-Avilés, “Raman characterization of carbon nanofibers prepared using electrospinning,” Synthetic Metals, vol. 138, no. 3, pp. 423–427, 2003. View at Publisher · View at Google Scholar · View at Scopus
  49. T. Hyeon, S. S. Lee, J. Park, Y. Chung, and H. B. Na, “Synthesis of highly crystalline and monodisperse maghemite nanocrystallites without a size-selection process,” Journal of the American Chemical Society, vol. 123, no. 51, pp. 12798–12801, 2001. View at Publisher · View at Google Scholar · View at Scopus
  50. M. Hanesch, “Raman spectroscopy of iron oxides and (oxy)hydroxides at low laser power and possible applications in environmental magnetic studies,” Geophysical Journal International, vol. 177, no. 3, pp. 941–948, 2009. View at Publisher · View at Google Scholar · View at Scopus
  51. D. L. A. De Faria, S. Venâncio Silva, and M. T. De Oliveira, “Raman microspectroscopy of some iron oxides and oxyhydroxides,” Journal of Raman Spectroscopy, vol. 28, no. 11, pp. 873–878, 1997. View at Publisher · View at Google Scholar · View at Scopus