Synthesis and Characterization of Silver-Containing Nanocomposites Based on 1-Vinyl-1,2,4-triazole and Acrylonitrile Copolymer

Table 1

Conditions of the synthesis of nanocomposites with 23.5% silver at a temperature of 210, 230, and 250°C.

No.	Time (min)	Crystalline phase	Degree of crystallinity (%)	The average size of crystallites (Å)	Weight loss (%)
210°C
1	5	—	—	—	—
2	15	—	—	—	—
3	30	Ag	11.5	46.2	2.7
4	45	Ag	16.3	58.4	3.6
5	60	Ag	23.2	68.9	5.2
6	90	Ag	38.9	80.1	14.7
230°C
7	5	—	—	—	—
8	15	Ag	33.9	55.1	10.2
9	30	Ag	58.0	75.6	34.3
250°C
10	2	—	—	—	—
11	5	Ag	46.0	90.0	22.1
12	15	Ag	63.8	114.8	40.7
13	30	Ag	73.0	125.6	48.8