Table of Contents Author Guidelines Submit a Manuscript
Volume 14, Issue 1, Pages 35-40

Total assignment of the 1H and 13C NMR spectra of piperovatine

Willy Rendón,1 Galia Chávez,1 Myriam Meléndez-Rodríguez,2 and Pedro Joseph-Nathan2

1Instituto de Investigaciones Químicas, Universidad Mayor de San Andrés, La Paz, Bolivia
2Departamento de Química, Centro de Investigación y de Estudios Avanzados, Instituto Politécnico Nacional, Apartado 14-740, México, D.F., 07000, Mexico

Copyright © 1998 Hindawi Publishing Corporation. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.


Total and unambiguous assignment of the 1H NMR spectrum of piperovatine [6‒(4‒methoxyphenyl)‒N‒(2‒methylpropyl)‒2,4‒hexadienamide] was carried out using conventional 1D NMR methods and spectral spin–spin simulation. Based on these data, the complete assignment of the 13C NMR chemical shift values was made by a 13C/1H chemical shift correlation diagram and conventional considerations for the quaternary carbon atom.