Research Article

Midinfrared FT-IR as a Tool for Monitoring Herbaceous Biomass Composition and Its Conversion to Furfural

Table 4

Ternary mixtures compositional data of a raw giant reed sample (stem + leaf) and of its solid residues coming from the hydrolysis reaction, by adopting different reaction temperatures. Reagents and operating conditions: 0.35 g of biomass, 0.10 mL of HCl 37 wt%, and 5.0 g of water. Ramping time = 5 min. All tests were performed in a CEM Discover S-Class MW reactor. Furfural yield is calculated as furfural Yield (wt%) = [furfural recovered after hydrolysis reaction (g)/dried starting biomass (g)] × 100. Solid residue yield is calculated as solid residue yield (wt%) = [solid recovered after hydrolysis reaction (g)/dried starting biomass (g)] × 100.

Giant reed sampleTemperature (°C)Cellulose (%)Hemicellulose (%)Lignin (%)Furfural yield (wt%) Solid residue yield (wt%)

Untreated41.623.624.6
1_112045.218.329.11.682.1
1_214055.96.232.19.369.8
1_315057.52.035.37.466.0