Research Article
Development of Flow Injection Spectrophotometric Method for 1-Napthylthiourea Using Sodium Nitrite and Sulphanilic Acid Diazotization Reaction
Table 1
Effect of physical variables on the determination of ANTU (
).
| Physical variables | Range studied | Optimum |
| Flow rate (mL/min) | 0.2–1.2 | 0.5 | Sample injection volume (µL) | 60–360 | 300 | Reaction coil-I length (cm) | 0–300 | 200 | Reaction coil-II length (cm) | 0–300 | 150 | Reaction coil-I and -II temperature (°C) | 10–50 | 30 |
|
|