Research Article

LC-QTOF-MS Analysis and Activity Profiles of Popular Antioxidant Dietary Supplements in Terms of Quality Control

Table 1

The declared ingredients of investigated dietary supplements.

Composition of the supplement (1 capsule/tablet)FormulationRecommended daily dose
IngredientsMass [mg]

S1 (turmeric)Turmeric rhizome powder720Capsule2

S2 (bilberry)Powdered bilberry fruit250Tablet2
Extract of bilberry including the following:40
(i) Anthocyanins10
(ii) Vit. C40
(iii) Vit. E6
(iv) Lutein3
(v) Beta carotene83.5

S3 (blend of extracts)Extract from the root of Baikal skullcap150Capsule2
Powdered cinnamon bark60
Cranberry fruit extract50
Extract from green tea leaves50
Extract of the herb of horsetail45
Vit. C40
Extract of chokeberry20
Extract from rhizomes of ginger12
Extract of bilberry fruit10
Extract of grape fruit3

S4 (acai)Extract of acai berry300Capsule1

S5 (grapes)Grape skin extract including400Capsule1
(i) Trans-resveratrol200
Grape seed extract including100
(i) Proanthocyanidins95

S6 (resveratrol)Resveratrol (from an extract of Reynoutria japonica)50Capsule1

S7 (Schisandra)Powdered fruits of the Schisandra chinensis525Capsule

S8 (goji)Extract of goji fruit including300Capsule1
(i) Polysaccharides150

S9 (pomegranate)Pomegranate peel extract including300Capsule1
(i) Elagic acid120

S10 (spirulin)Spirulin powder450Capsule3–6

S11 (green tea)55% green tea extract including the following:250Capsule1-2
(i) EGCG (epigallocatechin gallate)137.5
(ii) Polyphenols249
(iii) Catechins200

S12 (green coffee)Extract of green coffee including the following:800Capsule1
(i) Caffeine34.8
(ii) Chlorogenic acid400

S13 (hawthorn)Powdered fruit of hawthorn565Capsule1-2

S14 (OXXYNNEA and blend of extracts)OXXYNNEA200Capsule1
Grape seed extract (95% of proanthocyanidins)150
Extract from green tea leaves (55% of EGCG)150
Citrus bioflavonoids 40%150
Trans-resveratrol100
Extract of Rhodiola rosea root (4% of rosavins)100
Quercetin100
Extract from the leaves of artichoke (5% of cynarin)50
Extract of cranberry fruit (10% of proanthocyanidins)40
Alpha-lipoic acid30
Coenzyme Q1015
Astaxanthin5
Lycopene1
Beta carotene1

S15 (green coffee)An extract of green coffee beans (50% of chlorogenic acid) including400Capsule2
(i) Caffeine20

S16 (Ecklonia)Ecklonia cava extract 25 : 1 (98.8% pure Ecklonia cava—the stem and leaves standardized to 15% polyphenols and phlorotannins)53Capsule1

The fillers and additives forming capsule/tablet were omitted; OXXYNNEA—the blend of extracts of fruits and vegetables: white and red grapes, oranges, grapefruit, blueberry, papaya, pineapple, strawberries, apples, apricots, cherries, black currants, tomato, carrot, green tea, broccoli, cabbage, onions, garlic oil, wheat germ, cucumber, and asparagus.