Quantitative Analysis of Oxygen Gas Exhausted from Anode through In Situ Measurement during Electrolytic Reduction

<div>Schematic of the OR apparatus used for this study: (a) outer view (①: furnace, ②: outer STS crucible, ③: inner STS crucible, ④: top flange, ⑤: cathode, ⑥: anode, ⑦: reference electrode, ⑧: electrical insulator, ⑨: thermocouple, ⑩: Ar inlet, and ⑪: bottom) and (b) flow of incoming Ar and evolved gas (Ar + O<sub>2</sub>) through the top flange.</div>

Science and Technology of Nuclear Installations

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Figure 2

Figure 2: Quantitative Analysis of Oxygen Gas Exhausted from Anode through In Situ Measurement during Electrolytic Reduction 