Abstract

The purpose of this paper is to study the crack initiation, propagation, and coalescence of the sandy mudstone sample with two sets of prefabricated cross-flaws under uniaxial compression. This study is different from previous studies on single or multiple parallel prefabricated flaws. The prefabricated cross-flaws are characterized by the dip of the rock bridge with the direction of the main flaw () and the angle between the direction of main and minor flaws (). The effects of these two parameters on crack initiation, propagation, coalescence, crack initiation stress, and coalescence stress are analyzed. Moreover, numerical simulation of the uniaxial compression experiments is performed using PFC2D with a flat-joint model, and the simulation results are in good agreement with those from the experiments. The results demonstrate that the dip angle of the rock bridge with the direction of the main flaw () has strong effects on the crack initiation and coalescence stresses. The larger the angle between the direction of main and minor flaws , the greater the crack initiation and coalescence stresses. The crack initiation stress is reduced for the case with cross-flaws compared with that with non-cross-flaws. Meanwhile, the connection type of main flaws and the width of the crack coalescence zone are difficult to observe through the experiments and are discovered from the numerical simulation.

1. Introduction

Faults and joints in rocks affect the mechanical properties of rocks. Therefore, it is of great significance to study the initiation and propagation modes of cracks in rocks for the failure mechanism of rocks [1]. The study of the rock failure process mainly includes three aspects: experiment, theory, and numerical simulation.

In order to study the crack evolution mode during the failure of crystalline rock materials, many researchers have conducted laboratory experiments with rock materials such as resin, plexiglass, or gypsum and analyzed the initiation, propagation, and coalescence of wing cracks and secondary cracks which lead to the macroscopic failure of brittle materials [2]. These prismatic samples of rock-like materials which are usually prefabricated with one, two, or more cracks with different geometric parameters and are subjected to uniaxial compression test crack [3, 4], crack coalescence categories [46], crack initiation criteria [7, 8], and crack propagation patterns in different rock-like materials [9] were studied from different perspectives, which is helpful to the identification of rock cracks and the study of failure mechanism. Three types of cracks are observed during the rock failure process [4]: tensile cracks, mixed tensile-shear cracks, and shear cracks (Figure 1). The types and forms of crack coalescence are summarized through experiments and have been classified into nine categories [1012]. Open flaws and closed flaws had a substantial difference in terms of mechanical behaviors [12, 13]. The digital speckle correlation method [14], scanning electron microscopy, and environmental scanning electron microscopy imaging techniques [4], as well as active seismic monitoring [15] are applied to monitor the strain field of crack propagation. Hoek suggested that the crack propagation caused by the single crack could not explain the macrofracture in specimens [16]. Besides, compared with the effect of confining pressure (5–20 MPa), preexisting cracks have a greater impact on rock deformation, strength, and fracture coalescence [17]. In addition to the uniaxial compression test, the Brazilian split test of precracked specimens was also carried out to study crack propagation and coalescence [1822], by focusing on the effects of inherent rock properties. Three failure mechanisms are found in the shear test of discontinuous jointed granite, in which the shear properties and failure mechanisms are also analyzed [23]. In the above research, the cracks existing in the rock mass are simplified as straight cracks or pore cracks. However, some researchers believe that elliptical defects are also common types of defects in practical engineering. They studied the ultimate failure mode of sand specimens with two prefabricated elliptical defects [24]. Experimental studies on single ellipse defects show that the extension of tensile cracks around the pores of marble specimens is mainly affected by the nucleation and propagation of local strain zones [25]. Although in many studies in the past, various experiments and complex monitoring methods have been widely used. Real-time dynamic monitoring has extremely high requirements on the size and accuracy of the sensor and the method of CT scanning while loading is too expensive, so the available experimental methods are still not enough to explore the relevant micromechanisms.

The crack propagation in brittle materials with prefabricated flaws has long been explored using theoretical methods in the last century, and especially, many theoretical models for mixed-mode I-II crack initiation have been developed. Stress-based [2631], energy-based [3237], and strain-based [38, 39] are three main theories. The modified maximum-circumferential stress criterion, proposed based on the maximum circumferential stress, takes into account the changing elastoplastic boundary of the crack tip [40]. However, since these existing failure criteria are established based on tensile loads rather than compressive loads, these criteria are only valid in the positive region (crack opening). Therefore, they cannot predict fracture behavior in the negative region (crack closure). Numerical simulation methods are widely used in the study of crack propagation in rock materials and are especially suitable for situations that cannot be completed in the laboratory. The discrete element method is the most popular and general method for simulating crack propagation and coalescence in rock materials [41]. In the particle flow model, a bonded particle model (BPM) is proposed, which uses round or spherical particles in the dense accumulation of contact points representing the rock [42]. Based on the proposed BPM model, simulation about crack propagation and coalescence for many rocks have been carried out, which achieved consistent results as those obtained in the laboratory [4346]. Three inherent problems encountered in the application of the standard BPM model and their causes were also elaborated [47]. Simulation studies using the finite element method and nonlinear dynamics method show that, under different loading conditions, the mixed crack type, crack initiation sequence, and overall crack shape differ with the rock [48]. Besides, the boundary element method is proven by a study of comparing the experiment and numerical simulation of Brazilian splitting test to be efficient and easy, compared with PFC2D [19].

In summary, in experiments to study the propagation of cracks using rock-like materials with different proportions, as described above, cementation of particles in similar materials can result in a much lower ratio of compressive and tensile strength than in real rocks. In quarry simulations using the BPM model in PFC2D, the obstruction of the model itself to simulate particle locking also contributes to a lower rate of rock compression for tensile strength than natural rock materials. When the BPM model is used, (1) the ratio of unilaterally limited uniaxial compressive strength to tensile strength (UCS/TS) is unrealistically in the range of 3–7, (2) the internal friction angle is too low than the true value, and (3) the strength envelope line is linear, i.e., the Hoek–Brown (HB) strength parameter mi is small. The interface in the FJM model is resistant to rotation even after disconnection, whereas it is not in the standard BPM. Consequently, the BPM cannot be used to assess the impact of the compression/tensile strength ratio on crack propagation. Besides, the previous studies discussed above have mainly focused on single faults, double parallel faults, or multiple parallel faults, while in rock mass engineering with real fault, the faults are often crossed (Figure 2). Therefore, we present here an experimental and numerical study on transversal defects closer to the real situation. The uniaxial compression tests are performed first on samples of sandy clay containing two sets of transverse faults to examine the effects of the length of the rock bridge between the transverse faults,the angle between the main fault and the loading direction, and the inclination of the bridge of rock with the main fault, and the angle between the main fault and small defects in the propagation and fusion of cracks in defective rock masses. The Flat Joint Model (FJM) in PFC2D is then applied to simulate the uniaxial compression tests of rock samples with prefabricated transverse faults and to study the effects of different compression/tensile strength ratios on the type of crack and rock failure mechanism. New conclusions are drawn to provide a reference to elucidate the failure mechanism of rock masses with transversal faults.

2. Specimen Preparation and Apparatus

Sandy mudstone specimens (70 mm × 35 mm × 140 mm) were first prepared. Two holes were drilled in the rock sample (i.e., the intersection of the cross-flaws) with a round drill bit of 0.1 mm diameter, and based on this location, the cross flaws were cut with a wire saw. Each set of cross-flaws comprised a 12 mm-long main flaw and an 8 mm-long minor flaw. As illustrated in Figure 3, the distance between the endpoints of the rock bridge of the two main flaws is , and the main flaw is at 45° with the axial load. represents the angle between the directions of the main-flaw rock bridge and main flaw, namely, the dip of rock bridge, which varies from −60° to 120° at 30° intervals; is the angle between the directions of the main and minor flaws, i.e., 0°, 30°, 75°, and 90°. The combinations of the two geometric parameters eliminated yield of 11 specimens with the prefabricated cross-flaws (Table 1). An acoustic wave detector was used to remove rocks with large differences in wave velocity to ensure that the physical and mechanical properties of the specimen were as consistent as possible. Three replicates were prepared for each specimen, and a total of 33 specimens were used for uniaxial compression test. The specimens were named as follows: 30–45 represents the specimen with and .

To obtain the physical-mechanical properties of the sandy mudstone specimens, uniaxial compression and Brazilian splitting tests were conducted on cylindrical standard specimens (50 mm × 100 mm) [49]. Young’s modulus (), uniaxial compressive strength (UCS, ), Poisson’s ratio (), and uniaxial tensile strength (TS, ) of the specimens were obtained by averaging the results of five laboratory experiments (Table 2).

The uniaxial compression tests of the sandy mudstone specimens with the prefabricated cross-flaws were carried out using the MTS-816 electro-hydraulic servo-controlled rock mechanics testing system. During each test, crack initiation, propagation, and coalescence were recorded using a high-speed recording system (Figure 4). To ensure that the rock is tested in a quasi-static condition, displacement loading was applied at a loading rate of 0.002 mm/s [5] in the experiment, and the high-speed recording system captured 100 frames per second.

3. Experimental Results

This section can be divided into two sections as follows. In Section 3.1, the influence of the dip angle of the rock bridge with main flaw of prefabricated cross-flaws on the crack propagation is obtained. In Section 3.2, the effect of the angle between main and minor flaws on crack initiation and coalescence are analyzed.

3.1. Effect of the Dip Angle of Rock Bridge with Main Flaw

To analyze the effects of the dip angle on crack propagation and coalescence (one-to-one correspondence with pictures of each group from left to right), was selected while changing the dip angle . The seven specimens photographed by the high-speed recording system are shown in Figure 5.

In the specimen (−60)–45, type III tensile cracks first occur at the left tip of the top main flaw as well as the right tip of the bottom main flaw (Figure 5(a)). Then, the secondary cracks are initiated at the left tip of the top main flaw. With increasing load, the secondary cracks begin to occur at the right tip of the top minor flaw as well as the left tip of the bottom minor flaw. Meanwhile, a tensile crack zone is generated in the middle of the rock bridge between minor flaws. The secondary cracks link to the tensile crack zone in the rock bridge between minor flaws under stress, causing crack coalescence in category VII. The type III stretch cracks initiated at the right tip of the bottom main flaw propagate and generate secondary cracks, which coalesce with the existing cracks, causing oblique shear failure.

In the specimen (−30)–45, type III tensile cracks are first, which link up the main and minor flaws (Figure 5(b)). Additionally, type I tensile cracks are initiated at the right tip of the minor flaw, whereas type III tensile cracks are generated at the left tip of the top main and minor flaws as well as the two tips of the bottom main and minor flaws. With increasing axial load, mixed tensile-shear cracks occurs, whereas the secondary crack occurs in the middle of the rock bridge between the two minor flaws, causing U-shaped coalescence cracks. Eventually, tensile failure occurs in the specimen.

In the specimen (–30)–45, type III tensile cracks are first initiated, which link to the main flaw and grow upward (Figure 5(c)). Type I shear cracks are initiated at the right tip of the top main flaw, whereas the secondary cracks occur at its left top. Meanwhile, the secondary cracks are generated at the right tip of the bottom minor flaw. With increasing load, tensile cracks are formed in the middle of the rock bridge between minor flaws, which link to the secondary cracks under stress, causing crack coalescence in category II. Meanwhile, type I shear cracks also occur at the left tip of the bottom minor flaw and then propagate, leading to Y-shaped tensile-shear failure in the rock.

In the specimen (–30)–45 (Figure 5(d)), mixed tensile-shear cracks are first generated at the right tip of the top main flaw. Then, type II tensile cracks are initiated at the left tip of the bottom minor flaw and propagated upward. With increasing load, type III tensile cracks also occur at the left tip of the bottom minor flaw. A tensile crack zone appears in the middle of the rock bridge and eventually connects with the secondary cracks, leading to crack coalescence in category II. Finally, the failure mode of the specimen is a tensile-shear mixed-mode failure.

In the specimen 60–45, type III tensile cracks are first initiated (Figure 5(e)). Then, the secondary cracks are generated in the middle of propagating cracks. Type III shear cracks are initiated near the lower tip of the top main flaw. Additionally, type I tensile cracks occur at the lower tip of the top main flaw, and mixed tensile-shear cracks are initiated at the upper tip of the bottom main flaw; these cracks are linked up in the rock bridge region between the two main flaws, leading to crack coalescence.

In the specimen 90–45, type III tensile cracks are first initiated (Figure 5(f)), while type II shear cracks are generated along the direction of the main flaw. Subsequently, type III tensile cracks are initiated at the left tips of the bottom and top main flaws, and the secondary cracks are initiated at the end in both cases. Crack coalescence is completed through propagation, and linking of the secondary cracks is initiated at the two tips of the top and bottom minor flaws under stress, which is classified into category V.

In the specimen 120-45 (Figure 5(g)), type III tensile cracks are first initiated at the right and left tips of the top main and minor flaws. With increasing load, mixed tensile-shear cracks occur at the left tip of the top minor flaw, whereas at the left tip of the bottom main flaw, type I tensile cracks are generated downward and type III shear secondary cracks are initiated toward the upper left. These cracks propagate and coalesce on the left of the rock bridge between main flaws. This crack coalescence is classified into category VII, and the specimen shows tensile-shear failure in an inverted ┓ shape.

Comparison among Figures 5(a)5(g) reveals that, for , the specimens show pure shear failure; when is changed to –30°, the failure mode shifts to tensile failure, with cracks first initiated at the tip of the main flaw. When , the failure mode changes to tensile-shear mixed-mode failure, and the cracks begin to occur from the minor flaw. All cracks are initiated from the minor flaw for , and the number of crack types is the largest for .

3.2. Effect of the Angle between Main and Minor Flaws

To evaluate the effects of the angle on crack propagation and coalescence (one-to-one correspondence with pictures of each group from left to right), was selected while changing . The four specimens for different photographed by the high-speed recording system are shown in Figure 6.

In the specimen 30-0 (Figure 6(a)), the main flaw overlaps with the minor flaw; therefore, the specimen contains two prefabricated parallel flaws. Type III tensile cracks are first initiated at the right tip of the top flaw and the left tip of the bottom flaw and then propagated in opposite directions. Additionally, the secondary cracks begin to occur near the flaw tip in the rock bridge region, leading to crack coalescence in category I. The specimen eventually shows tensile-shear failure.

In the specimen 30-30 (Figure 6(b)), type III tensile cracks are first initiated at the right tip of the top main flaw, followed by the initiation of type I shear cracks. The secondary cracks are generated at the tips of the top and bottom main flaws, which are linked up in the rock bridge region to cause crack coalescence in category I. The specimen shows oblique shear failure.

In the specimen 30–75 (Figure 6(c)), type III tensile cracks are first initiated at the right tip of the top main and minor flaws and the left tip of the bottom main and minor flaws. These cracks are subsequently linked up; type I shear cracks are generated in the middle part of the linked tensile cracks and then propagated under stress. Type I shear secondary cracks begin to occur at the tip of the main flaw close to the rock bridge, which are linked up in the middle part of the rock bridge, leading to crack coalescence in category I. The specimen finally presents oblique shear failure.

In the specimen 30–90 (Figure 6(d)), type III tensile cracks are also first initiated at the left and right tips of the top main and minor flaws. With increasing load, type II shear secondary cracks are initiated at the tip of the main flaw near the rock bridge region, which leads to crack coalescence in category I. The specimen ultimately undergoes oblique shear failure.

The comparison among Figures 6(a)6(d) shows that the specimens undergo tensile failure for , whereas the failure mode changes to shear failure for ; this indicates that cross-flaws play a role in altering the failure mode of rock masses. Irrespective of the angle , the crack coalescence pattern of rocks always belongs to category I; this suggests that has no effect on the category of crack coalescence.

4. Numerical Simulation

4.1. FJM Model

The flat-joint contact and corresponding flat-jointed material are illustrated in Figure 7. Flat-joint contact simulates the interface behavior between two theoretical surfaces, and each surface is rigidly connected to an entity. A flat-joint contact material includes the entity (ball, cluster of particles, or wall) connected by the flat-joint contact so that the effective surface of each entity is defined by the notional surfaces of its various parts. These surfaces at each flat-joint contact interact with the notional surfaces of the contact entities. The notional surface is referred to as the facet, which is a line in two dimensions and a disc in three dimensions. The FJM model can be installed at the ball-ball and ball-facet contact. We regard the ball of flat-jointed material as a planar particle, each of which is depicted as a disc in two dimensions and a sphere with skirted faces in three dimensions. Further details about the FJM model concept can be found in the literature [50]. When the FJM model is installed at the point of ball-ball contact, faced grains are generated. There is an interface between each set of adjacent faces, which is discretized into elements. The interface discretization is controlled by the number of equal-length elements in the radial direction. Each of the elements is either bonded or unbonded. The fracture of each bonded element would cause a partial damage to the interface, and each fracture event represents a crack. If the relative displacement at the flat-joint contact is greater than the diameter of the flat joint, the adjacent faces can be removed (because the contact may be deleted), making the relevant ball partially circular in two dimensions and spherical in three dimensions. If these balls are recontacted, their behavior would contact (if the linear contact model is assigned to the new contact) between surfaces (disc in two dimensions and sphere in three dimensions).

The main microparameters characterizing the material constructed by the FJM model are provided in Table 3.

According to the size of sandy mudstone specimens (35 mm × 70 mm × 140 mm) used in the experiment (Section 2), rectangular cuboid model specimens containing two sets of cross-flaws were generated in the FJM model (Figure 8), with and being changed as in the experiments. The particle radius distribution ( and ) was selected according to the instructions of Itasca Company and previous studies [42, 45, 51].

4.2. Calibration of Microparameters

When applying the FJM model for numerical simulation, the microparameters need to be determined by parameter calibration. The trial and error method is most commonly used in calibrating the microparameters of the PFC2D model for rocks, that is, to continuously adjust the microparameters so that the numerical results are matched with the macromechanical properties of rocks. Here, we used Young’s modulus (), Poisson’s ratio (), uniaxial compressive strength (), tensile strength (), internal friction coefficient (), and cohesion strength () as the calibration criteria, which were obtained by uniaxial and biaxial compression tests and Brazilian splitting tests on sandy mudstone specimens.

The calibration results of the microparameters are provided in Table 3. The stress-strain curves from the uniaxial compression test are shown in Figure 9. A1–A5 are the stress-strain curves of five sandy mudstone specimens obtained by physical experiments, whereas the red line of the FJM is the stress-strain curve obtained by FJM simulation using the microparameters provided in Table 3. Clearly, the FJM model has captured most of the behaviors of sandy mudstone in physical experiments. Table 4 compares the macroparameters obtained by physical experiments and numerical simulation. The results of particle flow simulation are in good agreement with these of the physical experiments, which has verified the capability of the FJM for simulating sandy mudstone materials.

4.3. Simulation Results

Numerical simulations were conducted to model the experiments with , 0°, and 90° and , 30°, and 75° reported in Section 3.

4.3.1. Simulation About

Figure 10 shows the FJM model for , 0°, and 90° and associated photographs for crack initiation, propagation, coalescence processes, and fracture in experiment.

By comparing Figures 10(a)10(c), we find that when , the final failure of rocks generally shows a fracture in the connection direction of the two main flaws. However, when and 90°, there is a near-horizontal fracture. These results are consistent with the experimental data. Additionally, for , the types of cracks generated are most complicated, while the patterns of crack coalescence are diverse and the total number of cracks is also high. This indicates that crack propagation and coalescence in rocks are greatly affected by the dip of rock bridge, whereas the positional relationship of flaw distribution plays a considerable role in rock failure.

4.3.2. Simulation about

Figure 11 presents the FJM model for , 30°, and 75° and associated photographs for crack initiation, propagation, coalescence processes, and fracture in experiment.

As shown in Figure 11(a), when , the crack initiation force, peak strength, and crack coalescence force of specimens reach the maximum for all simulated specimens. This is because compared with non-cross-flaws, the presence of cross-flaws would further reduce the integrity of rock masses, resulting in a decline in their mechanical properties. In the experiments, only crack coalescence is observed in the middle of rock bridge, but the width of the crack coalescence zone cannot be observed. By contrast, the width of the crack coalescence zone is clearly seen in the simulation. When and (Figures 11(b)11(c)), the most bond fractures occur in the middle of rock bridge, which form the widest fracture zone. The corresponding rock fracture failure is more severe.

5. Discussion

To study the effects of and on crack initiation and coalescence stresses in rocks, we analyzed the experimental data and defined crack initiation and coalescence stresses as the stresses for new crack initiation and crack coalescence, respectively, as observed on the stress-strain curve (Lee and Jeon [9]).

5.1. Dip of Rock Bridge with Main Flaw

In the experiments on the specimens with different joint persistency, the stress measured by the testing system shows a slight drop and then continues to rise during crack initiation and coalescence (Figure 12). Points A, B, C, D, E, F, and G indicate the first stress drop on the stress-strain curve obtained in the uniaxial compression tests of rock specimens with , −30°, 0°, 30°, 60°, 90°, and 120°, respectively, which are the crack initiation stresses. Points H, I, J, K, L, M, and N indicate the corresponding second stress drop on the stress-strain curve, which are crack coalescence stresses. Because the specimens are real sandy mudstones rather than the rock made of rock-like materials, the strength of the specimens is not exactly identical due to heterogeneities. Thus, it makes little sense to simply compare the numerical values of the initiation and coalescence stresses. To reflect the effects of joint persistency on crack initiation and coalescence stresses in the rocks, the ratio [42, 45, 5155] was used to indicate the level of the crack initiation stress relative to the peak stress and the ratio to indicate the level of the crack coalescence stress relative to the peak stress, in which is the crack initiation stress, is the crack coalescence stress, and is the peak stress in the rock under axial compression. Based on the relationship of stresses at the points A–F and their respective peak stresses (Figure 12), the and ratios with three different are obtained (Table 5). The curves of versus and are shown in Figure 13.

The and ratios obtained at different are listed in Table 5. The ratio varies between 0.33 and 0.73, indicating the large effect of on crack initiation force. The ratio varies from 0.47 to 0.86. The curves of versus and are shown in Figure 13.

Both the and ratios increase first and then decrease with the increasing angle . Our results indicate that the angle controls the left-right positional relationship between the two sets of cross-flaws. This means the relative position of these cross-flaws has strong effects on the timing of crack initiation and coalescence. When varies from –60° to 30°, both the and ratios increase and their maximum reached at . When , both and become decreasing.

5.2. The Angle between Main and Minor Flaws

The stress-strain curves for different are analyzed following the method mentioned in Section 3.2 In Figure 14, A–E represent the crack initiation stresses of specimens for , 30°, 45°, 75°, and 90°; H–L represent the corresponding crack coalescence stresses. The and ratios obtained with different are listed in Table 6. The value is within the range of 0.31–0.51. The value is between 0.88 and 0.96, showing minor changes, which indicates that the angle between main and minor flaws has little effect on the crack coalescence stress. The curves of versus and are shown in Figure 15.

The and ratios increase with the increasing angle . For , the main flaw overlaps with the minor flaw, and there are only two parallel flaws in each rock specimen. In this case, the ratio is the highest, which indicates the crack initiation is closest to the peak stress and the initiation is more difficult for non-cross-flaws than for cross-flaws. When is not 0, the main flaw is crossed by the minor flaw, and the ratio increases with increasing angle. The lowest ratio is obtained for , which means the crack initiation is the earliest and easiest. The ratio has little change when varies from 30° to 75°, whereas a maximum is observed for . This trend indicates that increasing the angle between main and minor flaws has little effect on crack coalescence stress; however, the coalescence stress reaches its maximum when the main and minor flaws are perpendicular to each other. This is in agreement with our experimental observation (Figure 6(d)) that the cracks are first initiated at the tips of the main and minor flaws, and only after they are linked, crack coalescence occurs between the two sets of main and minor flaws.

6. Conclusions

In this study, uniaxial compression tests were performed on sandy mudstone specimens containing two sets of cross-flaws. The experimental processes were simulated by the FJM model based on PFC2D numerical simulation. Then, the effects of two geometric parameters on crack propagation, initiation stress, and coalescence stress were analyzed. The results indicate that the FJM model is robust to simulate the processes of crack initiation, propagation, and coalescence in sandy mudstone specimens. The key conclusions of this study are given below:(1)In the rock specimens with prefabricated cross-flaws, type III tensile cracks are the first cracks initiated in physical experiments and FJM simulation.(2)The dip of the rock bridge with main flaw () have strong effects on crack initiation and coalescence stress. The initiation and coalescence stresses increase first and then decrease with the increasing angle () in a parabolic pattern. Moreover, increasing the angle between main and minor flaws () results in higher crack initiation and coalescence stress, and the initiation force is reduced for cross-flaws compared with non-cross-flaws.(3)The angle () is the most influential geometric parameter for the rock failure mode and crack initiation, propagation, and coalescence. By comparison, the angle () has less effect on crack coalescence and failure mode.

Data Availability

The data used to support the findings of this study are available from the corresponding author upon request.

Conflicts of Interest

The authors declare that they have no conflicts of interest.

Acknowledgments

This work was supported by the National Natural Science Foundation of China (52034007 and 52074263) and National Key Research and Development Plan (2017YFC0603001).