Characterization of the Polycaprolactone Melt Crystallization: Complementary Optical Microscopy, DSC, and AFM Studies
Figure 8
(a) Rheological measurements of the polycaprolactone crystallization at 45°C: storage modulus G′, loss modulus G′′, complex viscosity , and temperature measured simultaneously under constant stress of 100 Pa and constant frequency of 0.1 rad/sec. (b) Rheological measurements of the polycaprolactone crystallization at 47°C: storage modulus G′, loss modulus G′′, complex viscosity , and temperature measured simultaneously under constant stress of 100 Pa and constant frequency of 0.1 rad/sec.
