Synthesis of Ti₂SnC under Optimized Experimental Parameters of Pressureless Spark Plasma Sintering Assisted by Al Addition

Figure 4

Effect of (a) sintering temperature holding time and (b) holding time on the peak ratio of Ti₅Sn₃/Ti₂SnC and Sn/Ti₂SnC at a molar ratio of 2 : 1 : 0.2 : 1 for Ti : Sn : Al : C.