Research Article

Efficient Synthesis and Characterization of Some Novel Nitro-Schiff Bases and Their Complexes of Nickel(II) and Copper(II)

Table 1

The results of the reaction for preparation of nitro-Schiff bases.

Entry 𝑅 (Scheme 1)LigandTime (min)Yielda (%)M.p (°C)

1(CH2)2L14091.0272–274
2(CH2)3L24090.0210–213
3(CH2)4L34588.5173–176
4(CH2)7L45588.0150–152
5(CH2)8L55585.0161–164
6701826.tab.001aL64592.0261–264
7701826.tab.001bL75592.0193–195
8701826.tab.001cL86094.0204–206

aIsolated yields.