Properties of Raw Saudi Arabian Grey Kaolin Studied by Pyrrole Adsorption and Catalytic Conversion of Methylbutynol
Table 1
Experimental conditions of pyrrole-TPD.
Pyrrole-TPD conditions
Description
Sample amount and particle size
0.3 g with a particle size distribution of 150–250 μm
Instrumented detector
Thermal conductivity detector (TCD)
Conditioning flow
Helium was utilized as carrier gas (50 mL/min), heated to 270°C, with a heating rate of 15°C/min. After that, a helium flow filled with pyrrole at 30°C was passed over the conditioned sample at a flow rate of 50 mL/min, for 30 min
Temperature-programmed desorption of pyrrole
Sample was then investigated up to 270°C with a heating rate of 15°C/min