Determination of Mycotoxins and Veterinary Medicines in Duck Flesh and Viscera and Assessment of Their Exposure
Table 2
Results for the recovery and precision arising from the validation of the analytical method.
Analyte
Medium
High
Low
Recovery (%) (n = 6)
Intraday precision (%) (n = 6)
Interday precision (%) (n = 6)
Recovery (%) (n = 6)
Intraday precision (%) (n = 6)
Interday precision (%) (n = 6)
Recovery (%) (n = 6)
Intraday precision (%) (n = 6)
Interday precision (%) (n = 6)
AFB1
91.3
5.82
6.38
105.9
8.90
7.83
95.6
3.61
8.91
AFB2
87.2
8.61
9.60
103.8
6.37
8.67
90.8
5.87
7.34
AFM1
103.7
7.31
6.83
93.7
6.96
9.18
87.3
9.18
9.66
T-2
87.6
5.86
10.61
92.6
7.82
9.60
87.5
10.60
5.87
OTA
90.5
7.90
9.61
89.1
9.10
8.17
91.3
9.24
8.20
ZEN
106.9
9.66
7.90
88.6
7.91
6.15
106.1
9.61
8.93
Levels used for precisions and recovery assays were level 1 = 5 μg/kg, level 2 = 40 μg/kg, and level 3 = 100 μg/kg for AFB1, AFB2, AFM1, OTA, T-2, and ZEN.
