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Advances in Materials Science and Engineering
Volume 2016, Article ID 2658621, 7 pages
Research Article

Preparation of Magnetic Hybrid Microspheres with Well-Defined Yolk-Shell Structure

1Hubei Collaboration Innovative Center for Nonpower Nuclear Technology, Hubei University of Science and Technology, Xianning 437100, China
2School of Nuclear Technology and Chemistry and Biology, Hubei University of Science and Technology, Xianning 437100, China

Received 15 June 2016; Revised 6 September 2016; Accepted 8 September 2016

Academic Editor: Peter Majewski

Copyright © 2016 Yuan Zhao et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.


A facile and efficient route was reported to prepare a kind of yolk-shell magnetic hybrid microspheres by suspension polymerization and calcinations method. The morphology, structure, and composition of the magnetic microspheres were characterized by FTIR, XRD, TEM, SEM, and TGA analysis. The vibrating-sample magnetometry (VSM) results clearly showed that the magnetic particles were superparamagnetic with saturation magnetization of 32.82 emu/g which makes the microcomposites easily controlled by an external magnetic field. The results revealed that the magnetic hybrid microspheres might have important applications in magnetic bioseparation and drug delivery.