Research Article

Quality Parameters, Volatile Composition, and Sensory Profiles of Highly Endangered Spanish Citrus Fruits

Table 4

Volatile compounds (%) in the juice of endangered Spanish sour (SoLi) and sweet (SwLi) limes and sweet lemon (SwLe).

CompoundRT (min)CodeANOVAContent (%)
SoLiSwLiSwLe

Hexanal7.36J10.22 a0.05 b0.28 a
E-2-Hexenal8.35JP10.07 b0.06 b0.28 a
Isoamyl acetate8.88J2NS0.05NdNd
Heptanal9.38J3NS0.02Nd0.03
α-Thujene10.18JP2NSNd0.020.17
α-Pinene10.49JP30.27 b0.20 b0.59 a
2-Heptenal11.08J4NS0.100.030.12
Sabinene11.66JP40.11 b0.58 ab0.78 a
β-Pinene11.97JP53.66 b4.35 b5.98 a
Octanal12.47JP61.40 a0.65 b0.79 b
Hexyl acetate12.56JP70.52 a0.02 b0.04 b
α-Terminene13.19JP8NS0.100.050.18
p-Cymene13.57J50.04 b0.03 b0.67 a
Limonene13.81JP944.7 b40.0 c56.6 a
β-Phellandrene13.88J6NS0.340.390.50
1,8-Cineole13.92J70.19 b0.16 b0.33 a
E-β-Ocimene14.03J80.35 a0.19 b0.23 ab
2-Octenal14.62J90.07 b0.02 b0.39 a
γ-Terpinene14.72JP100.41 b0.17 c6.03 a
1-Octanol15.23JP11NS0.040.020.02
Heptyl acetate15.47J10NS0.040.040.01
α-Terpinolene15.87JP120.44 a0.05 b0.31 a
Linalool16.49JP1319.9 b40.6 a2.74 c
Nonanal16.55JP140.20 c4.09 a1.06 b
Limonene oxide18.18J110.05 b0.04 b0.24 a
Citronellal18.55JP150.02 b0.10 b0.52 a
2-Nonenal18.96JP16NS0.04 b0.04 b0.25 a
Borneol19.32J12NS0.040.020.01
δ-Terpineol19.78JP17NS0.030.040.15
2-(2-Propenyl)-phenol19.87J13NS0.07Nd0.01
Terpinen-4-ol20.25JP181.08 a0.36 b0.86 ab
α-Terpineol20.96JP193.95 a1.07 c2.99 b
Neral22.63JP200.91 c1.57 b6.73 a
Linalyl acetate22.85JP2113.2 a0.36 b0.12 b
Carvone23.14JP22NS0.190.100.13
2-Decenal23.66JP23NS0.080.040.05
Geranial23.96JP241.55 b2.10 b8.28 a
Perillaldehyde24.73JP25NS0.080.180.14
Bornyl acetate24.91JP26NS0.110.170.01
Caryl acetate26.41J14NS0.280.350.76
Citronellyl acetate27.40JP27NS0.170.010.02
p-Menth-1-en-9-yl acetate acetate27.67JP28NS0.510.04nd
Neryl acetate27.89JP291.63 a0.01 b0.12 b
Geranyl acetate28.80JP301.96 a0.01 b0.04 b
Decyl acetate30.16JP31NS0.050.010.01
Dodecanal30.35JP32NS0.020.020.02
β-Bergamotene30.78JP33NS0.010.020.01
β-Caryophyllene31.43JP34NS0.070.140.07
α-Bergamotene31.67JP35NS0.300.450.14
α-Bisabolene34.54JP36NS0.040.050.04
β-Bisabolene34.92JP360.32 ab0.93 a0.15 b

NS = not significant at ; significant at , 0.01, and 0.001, respectively; values (mean of 3 replications) followed by the same letter, within the same row, were not significantly different , according to Tukey’s least significant difference test.