Research Article

Evaluation and Assessment of Aflatoxin M1 in Milk and Milk Products in Yemen Using High-Performance Liquid Chromatography

Table 1

Validation of detection protocol through recovery of known amount of mycotoxins in AFM1-free milk. AFM1-free samples were mixed with a known amount of AFM1 standard and analysed by HPLC.

Spike sampleHPLC peak areaRecovery (%)AFM1 con. in milk (ppb)

Sample 1116395108.310.541333 ± 1.01
Sample 2118984110.730.553441 ± 0.97
Sample 3110651102.940.514469 ± 0.96