Disperse Solid-Phase Extraction Cleanup for the Determination of 1-Deoxynojirimycin in Mulberry Leaves with Ultraperformance Liquid Chromatography-Tandem Mass Spectrometry

<div>Real sample test chromatograms for the quantitation ion of 1-DNJ with the four types of column (<i>c</i> = 500 ng/mL). Column 1: Agilent ZORBAX Eclipse Plus C18, 2.1 × 50 mm 1.8 <i>μ</i>m, column 2: Waters ACQUITY UPLC® BEH HILIC, 2.1 × 50 mm 1.7 <i>μ</i>m, column 3: SunShell C18, 4.6 × 100 mm 2.6 <i>μ</i>m, and column 4: Pinnacle II Amino, 4.6 × 150 mm, 3 <i>μ</i>m.</div>

Journal of Food Quality

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Figure 1

Figure 1: Disperse Solid-Phase Extraction Cleanup for the Determination of 1-Deoxynojirimycin in Mulberry Leaves with Ultraperformance Liquid Chromatography-Tandem Mass Spectrometry 

Figure 1 | Disperse Solid-Phase Extraction Cleanup for the Determination of 1-Deoxynojirimycin in Mulberry Leaves with Ultraperformance Liquid Chromatography-Tandem Mass Spectrometry 